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GCMS analysis results for sample AE11155, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11155 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024495–000024513

Folder label: “GCMS X 5/13/02 A 5/16/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020515\11155.D Vial: 21 Acq On : 16 May 2002 7:34 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Butane, 2,3-dichloro-2-methyl- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 5.65 2.70 ug/1 202899 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

’— 1 Butane, 2,3-dichloro-2-methyl- 140 C5H10C12 000507-45-9 72 2 Propane, 1,1-dichloro- 112 C3H6C12 000078-99-9 53 3 Propane, 2-bromo-l-chloro- 156 C3H6BrCl 003017-95-6 28 4 1 - Propene , 3 -chloro- 76 C3H5C1 000107-05-1 11 Abundance Scan 437 (5.647 min): 11155.D (-430) (-) m/ z 77.10 100.00% 41 77 A

5000 53 105 -HHl, । 63 89 .I l 125 207 \ 5.40 5.60 5.80 6.00 H TTuuDTTOTT m/z 41.10 96.25% m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #29395: Butane, 2,3-dichloro-2-methyl- 77

41 5000 T । ' ' ' i vtud । ' ■ 5.40 5.60 5.80 6.00 27 m/z 69.10 49.17% +444+++4+ |1111'89‘T ■ ■1 ′′′′′ 53 63 I no 105 •n-f |, 125 140 " ■ r ′′′ ।।>|i। 1' I" " r " ' i" " i" ■' i" " r nz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance

29 41 77 #29392: Propane, 1,1 -dichloro-

W 5.40 5.60 5.80 6.00 5000 m/z 76.00 38.35%

‘ I’’’ „ 51 61 , 187 97 112 Tmp 11 I'1 "I " "i'r"' r"' i""i"" I""I" "I"1 ■ r'" i""i"" i' n/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #115667: Propane, 2-bromo-1 -chloro- 77 5.40 5.60 5.80 6.00 m/z 79.10 38.31% 5000 41

27 .... I | 51 63 r 93 197 121 111" 1' - 143I 158 >।■■।111 >111 ■ ■■<।■1 • ।1111 r11111 ”11' n/z—> 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 5.40 5.60 5.80 6.00

11155.D SCAN020507.M Thu May 16 09:34:58 2002 Page 7

NYC-WTC_000024505

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NYC-WTC_000024505Source: NYC Law Department, mirrored locally

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