GCMS sample results AE11284, DEP Labs, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020516\11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) .. Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 8 Octane, 1,1’-oxybis- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 11.80 0.91 ug/1 52252 1,4-Dichlorobenzene-d4 11.37 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Octane, 1,1’-oxybis- 242 C16H340 000629-82-3 58 2 Nonane, 2,6-dimethyl- 156 C11H24 017302-28-2 50 3 Octane, 3-ethyl- 142 C10H22 005881-17-4 50 4 Octane, 3-ethyl- 142 C10H22 005881-17-4 50 Abundance Scan 1485 (11.804 min): 11284.D (-1477) (-) m/z 43.20 100.00% 43 57 71

50001

85 119 nonuw VA 11.40 11.60 11.80 12.00 12.20 nz-> TT-p-n-r-p 20 40 Il 11 ' I ■ ' 60 l44 80 ' i 1 1 ■ ‘ i ' ■ ■ ■ i 1 ■ ■ ■ i ■ • ' • i ■ 1 1 ■ i ■ ■ 100 120 140 160 180 200 220 240 m/z 57.10 89.88% Abundance #17060: Octane, 1,1’-oxybis- 57 71 43 5000 w MyLenpoud 11.40 11.60 11.80 12.00 12.20 84 m/z 71.10 83.15% 29 1 112

miz-> .1544 20 40 rr T7 — 60 80 97 | 131143 100 120 140 160 180 200 185 199 220 243 240 Abundance #5582: Nonane, 2,6-dimethyl- 43 57 71 AMMAboALnulat 11.40 11.60 11.80 12.00 12.20 5000 m/z 55.10 41.17%

29 85 449

miz-> — 20 40 U60 ?||| 1 OT J']0 127 141156................ 80 100 120 140 160 180 266' '226' 240 Abundance #5609: Octane, 3-ethyl- 43 57 11.40 11.60 11.80 12.00 12.20 71 m/z41.10 40.23% 5000 29 112 1 ' 1 4 FTTII, ’ I,1 1111 .83 ' 981...... 142............................... 1 ■ ■ i ■ •1 l ■ •' ■ i ■ • ' ■ ■ • • i > ■ ■ i i ■ ‘ ■ i ■ ■ ,-rt i1 ' ■ ■ ■ i ■ n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 11.40 11.60 11.80 12.00 12.20

11284.D SCAN020507.M Fri May 17 13:06:41 2002 Page 11

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