GCMS sample results AE11284, DEP Labs, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020516\11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) , Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 9 Naphthalene, 1,2,3,5,8,8a-h... Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 12.79 0.64 ug/1 36536 1,4-Dichlorobenzene-d4 11.37 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Naphthalene, 1, 2,3,5,8,8a-hexahy... 134 C10H14 062690-65-7 43 2 Bicyclo[4.2.o/oct-l-ene, 7-exo-e... 134 C10H14 1000142-18-2 43 3 Bicyclo[4.2.0]oct-1-ene, 7-endo-... 134 C10H14 1000142-18-3 38 4 Cycloheptane, l,3,5-tris(methyle. . . 134 C10H14 068284-24-2 38 Abundance / Scan 1652 (12786 min): 11284.D (-1643) (-) m/z 105.10 100.00% 105 91

5000 41

T-7-r-r-rT-TT-rrn-Y^-^^ 51 57 67 77

IP 119 134 111 • • • • i •1 ■11 • A/. N 12.40 12.60 1280 13.00 13.20 m/z 91.10 82.75% nz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #38307: Naphthalene, 1,2,3,5,8,8a-hexahydro- 91

_A L 134

5000 79 105 119 12.40 12.60 12.80 13.00 13.20 41 m/z 92.10 57.43% 27 51 65 — ++ I1! । ■ Il,F7 11111,73 185. — --11 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140’ Abundance #37361: Bicyclo[4.2.0]oct-1-ene, 7-exo-ethenyl- 91 • i ■ ' /1.1.... ‘ ‘ I 1 * ‘ * I ‘ ‘ 12.40 12.60 12.80 13.00 13.20 ‘ J ' 1

5000 m/z 67.20 41.88% 79

-+ 39 105 119 51 65 134 — 584— MAAun/Maai • I 1 »’*'> I ■' । 11 i'l l 11 । > । t' It n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #37362: Bicyclo[4.2.0joct-1-ene, 7-endo-ethenyl- 9h 12.40 1260 12.80 13.00 13.20 m/z 119.20 39.55% 5000 79 39 105 119 134 51 65 11 n''"' l ' ■ " —1458,4.1, • ‘14 111 ‘ 1 i 1 ,'1'' I ■ ‘ ■ ■ i ■' -AP niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 12.40 12.60 12.80 13.00 13.20

11284.D SCAN020507.M Fri May 17 13:06:41 2002 Page 12

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