GCMS sample results AE11284, DEP Labs, June 2002

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Data File : C:\MSDCHEM\1\DATA\020516\11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) . Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 10 Benzene, 1-methyl-3-propyl- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 13.04 0.84 ug/1 48253 1,4-Dichlorobenzene-d4 11.37 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, 1-methyl-3-propyl- 134 C10H14 001074-43-7 83 2 Benzene, 1-methyl-2-propyl- 134 C10H14 001074-17-5 72 3 Benzene, 1-methyl-3-propyl- 134 C10H14 001074-43-7 72 4 Benzene, 1-methyl-3-propyl- 134 C10H14 001074-43-7 72 Abundance Scan 1695 (13.038 min): 11284.D (-1683) (-) m/z 105.10 100.00% 105

5000

43 77 134 1

niz-> Abundance ' ■ ■ I ■ ■ ' ‘ I 1 1 ' ' I' 10 20 30 —L AA4 40 TT 50 60 70 #119326: Benzene, 1-methyl-3-propyl- 80 91 115 I i_______ ' i ■ • ■' I ■ ■ • ■ i ■ 90 100 110 120 130 140 1...... * ‘ J ‘ ‘ 12.80 13.00 13.20 13.40 m/z 134.10 23.01%

105

5000| f 1 ■ i ■ ■ ■ • i • ' 12.80 13.00 13.20 13.40 134 m/z 77.20 21.44% 77 91

miz-> 10 20 30 40 50 L 80 90 100 110 120 130 140 60 70 -pPPPP ’ I’* 119

Abundance #119333: Benzene, 1-methyl-2-propyl- 105 12.80 13.00 13.20 13.40 5000 m/z 43.05 19.55% 134 27 39 F. er d/ 91 51 58 65 11 I 115, 127 +**’1***1144 111111 • r' —mthmmP 1111 ''' I''1111 ■ ■ i ■ • _______________ L______ i, n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #46925: Benzene, 1-methyl-3-propyl- *I*11**IIII1"I 105 12.80 13.00 13.20 13.40 m/z 106.00 15.84% 5000

134 15 27 39 51 63 77 91 1 -It_________ . I ■ I_________ _ ____________ .1.1 11161** I » I » I > 11’4 1 * 1 |Irrs I 1*1 1 I J I l ++84-1,98,1 119 127 ___ _ 111 ‘"i ■ ■" i1 ■ • i • • m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 12.80 13.00 13.20 13.40

11284.D SCAN020507.M Fri May 17 13:06:41 2002 Page 13

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