GCMS results for sample AE11566, May 29, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020521\11566.D Vial: 17 Acq On : 22 May 2002 12:10 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Benzene, 1,2,3,5-tetrachlor... Concentration Rank 4 R.T. EstConc Area Relative'to ISTD R.T. 28.91 0.24 ug/1 25215 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, 1,2,3,5-tetrachloro-4,6... 242 C8H6C14 000877-09-8 38 2 Benzene, l,3,5-trichloro-2-(1-me... 222 C9H9C13 054965-70-7 27 3 Benzene, 1,4-bis(dichloromethyl)- 242 C8H6C14 007398-82-5 12 4 Quinoline, 3 -bromo- 207 C9H6BrN 005332-24-1 9 Abundance / Scan 4396 (28.908 min): 11566.D (-4387) (-) m/z 209.00 100.00% 209 244

5000 84 102 ............... ...... ................................ 44 55 138 73 172

miz-> 0- 20 40 || iLl 1 i ■ ■ ' 1 i 60 80 III.... 100 120 140 160 180 200 * | ' T7 ■ ■ ' . ( r-i ! . | 220 240 28.60 28.80 29.00 29.20 m/ Z 2 07.00 71.99% Abundance #84890: Benzene, 1,2,3,5-tetrachloro-4,6-dimethyl- 207 244 5000 136 1 1/4111 14‘ 28.60 28.80 29.00 29.20 11 m/z 244.00 68.60% 51 74 85 99 171

niz-> 0- AL20 40 60 80 100 120 Tp . 157 , 193 I 229 „ ■H-r 140 160 180 200 220 240 Abundance #84887: Benzene, 1,3,5-trichloro-2-(1-methylethyl)- 207 1 1 I 1 1 1 1 I 1 ' ' I ' ' ' 1 I ' ' ' ' I 28.60 28.80 29.00 29.20 5000 m/z 245.80 44.35% 222 136 171 194 0- , 27 41 । । । । 'i , p/ = 68 85 99 115 1147159 41824 T"—PP— r mp ll, । he plll,—hp—r r i f n1111 r■ nZz-> Abundance 20 40 60 80 100 120 140 160 180 200 2201 #84882: Benzene, 1,4-bis(dichloromethyl)- 172 207 240 I.. Ill...... 28,60 28.80 29.00 29.20 m/z 84.10 30.58%

5000 101 51 75 86

0 27391631,44,4412125/1/149159.4 ' 'I ' ' ■ ■ 1 1 1 137 —— — 244 — 4, ■ ' T.I n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 28.60 28.80 29.00 29.20

11566.D SCAN020521.M Fri May 24 09:40:06 2002 Page 4

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