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GCMS analysis results for sample AE11278, May 2002

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Laboratory report documenting GCMS analysis of sample AE11278 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024692–000024705

Folder label: “GCMS X 5/13/02 A 5/15/02

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NYC 9/11 Public Portal Document Library search Compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11278.D Vial: 12 Acq On : 15 May 2002 10:41 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Benzene, 1,2,3,5-tetrachlor... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 28.91 0.22 ug/1 23463 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, 1,2,3,5-tetrachloro-4,6... 242 C8H6C14 000877-09-8 59 2 4-Amimo-5-[3,4-dichlorophenyl]-2... 244 C8H6C12N4O 1000213-70-9 14 3 7-ChLoro-4-methoxy-3-methylquino... 207 C11H10C1NO 1000213-52-2 9 4 1-Pentanamine, N-butyl-N-nitroso- 172 C9H20N2O 016339-05-2 9 Abundance Scan 4396 (28.908 min): 11278. D (-4387) (-) m/z 206.90 100.00% 207 244 5000 86 136 172

54 68 ...... I bl. n/z-> —LLL 40 60 80 110

■11' ‘ ‘111 i1' ■ ■ i11 ■ । ■ i ■ 'i > । > । ■ 11 100 120 140 160 180 200 220 240 260 280 300 320 327 ........................... | 28.60 28.80 29.00 29.20 m/z 209.10 72.61% Abundance #84890: Benzene, 1,2,3,5-tetrachloro-4,6-dimethyl- 207

5000 136 244 L 28.60 28.80 29.00 29.20 51 85 99 171 m/z 244.10 63.95%

/z—> J, . 1681 , i 1121 h 157 ,|||, 193 229 "’IT . ...I 1 1 1 1 11 1 1 T 1 ' 1 1 1 1 1 1 1 1111' 111111 1 1 1 1 1 1 '11 ■ ■ ' ■ i i ■ ■ i > ■ ■ ■ i ■ ■ ■ ■ i ■ । ■ i ■ ■ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 I Abundance #92155:4-Amino-5-[3,4-dichlorophenyl]-2,4-dihydro-3H-1,2,...

172 244 . All.. 28,60 28.80 29.00 29.20 5000 m/z 245.80 52.83% 44 145 75 100 124

iz-> 40 61 —. Ihall-r 4- |ll r l .[ l, 1 r 4 qu"r 60 80 100 120 140 160 r 44187 ++ 180 .1,22 200 213 8,, 260 280 220 240 300 320 J Abundance #84815:7-Ch)oro-4-methoxy-3-methylquinoline ' 1 I 1 1 1 1 I ' ' ■ I ' ' ' ' I ' 1 ' ‘ I 207 28,60 28,80 29.00 29.20 178 m/z 136.00 49.33% 75 5000

51 102 138 164 192 ............................. ........................

n/z-> 4llaka,44m+*4+ 40 60 80 TI’ 100 120 140 160 180 200 220 240 260 280 300 320 T’11:1"1111117*1101111133111 28.60 28.80 29.00 29.20

11278.D SCAN020507.M Thu May 16 09:56:22 2002 Page 6

NYC-WTC_000024701

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NYC-WTC_000024701Source: NYC Law Department, mirrored locally

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