Laboratory report of GCMS analysis for sample AE11425 conducted on May 29, 2002.
NYC-WTC_000022526–000022538Folder label: “GCMS X 5/17/12 A 5/21/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C : \MSDCHEM\ 1 \DATA\ 020521 11425.D Vial: 11 Acq On : 21 May 2002 6:15 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Benzene, 1,2,3,5-tetrachlor... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 28.90 0.21 ug/1 22198 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzene, 1,2,3,5-tetrachloro-4,6... 242 C8H6C14 000877-09-8 37 2 3-(Trichlorovinyl)pyridine 207 C7H4C13N 1000140-10-7 27 3 Benzene, 1,4-bis(dichloromethyl)- 242 C8H6C14 007398-82-5 27 4 Benzofuran-2-one, 2,3-dihydro-3 , . . . 207 C10H9NO4 1000129-53-4 27 Abundance Scan 4395 (28.902 min): 11425.D (-4387) (-) m/z 207.00 100.00% 172 207 136 49 63 75 86 244 5000 110 193 227 4 ‘ ■ i 1 ‘ • i 28.60 28.80 29.00 29.20 Of 1*——/ m/ Z 2 09.00 95.66% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #84890: Benzene, 1,2,3,5-tetrachloro-4,6-dimethyl- 207
244 5000 . .1......4,...... 136 28.60 28.80 29.00 29.20 m/z 172.00 90.61% 51.74 85 99 171 ..... IM? l/110121 0 i 1 r 1 1 I 1 11 1 |1 1 11 i11 1 1 i1 T1 1 r"' 1 1 III , 157 a 193 , 229 h Ir m/z-> 20 40 60 80 100 120 140 160 . 180 200 220 240 Abundance #74994:3-(Trichlorovinyl)pyridine 172 • 1 i ■ 1 ■ ■ i ■ ■ mI 28.60 28.80 29.00 29.20 78 m/z 136.00 66.47% 5000 52 207 137
iz-> 0 20 40 ‘IB 60 —l—M2 80 100 120 140 160 180 200 hi - - 220 240 Abundance #84882: Benzene, 1,4-bis(dichloromethyl)- 172 207 28.60 28.80 29.00 29.20 m/z 244.00 55.06% 5000 101 51 75 86 137 244 0 27 39 J I ■ ' 1 1 i ' 1 tr at 112 125.4 148159 J "mi 1 n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 28.60 28.80 29.00 29.20
11425.D SCAN020521.M Fri May 24 09:26:47 2002 Page 6
NYC-WTC_000022535
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NYC-WTC_000025520
Laboratory report of GCMS analysis for sample AE10812 conducted on May 29, 2002, showing surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024652
GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025542
Laboratory report documenting GCMS analysis of sample AE11154 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022561
Laboratory commentary noting no unusual compounds detected in the GCMS scan of sample AE11480 on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025568
GCMS analysis report for sample AE11567 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025613
GCMS analysis report for sample AE11571 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043779
Analytical report for sample AE09767 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045748
Gas chromatography-mass spectrometry analysis of sample AE10701 conducted May 20, 2002, detecting unknown compounds and 2,4-DDD at 82% recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046192
Gas chromatography-mass spectrometry analysis of sample AE10135 performed May 17, 2002, detecting unknown compounds and 2,4-DDD surrogate at 96% recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046147
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10132 on May 17, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043806
Analytical report for sample AE09769 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000022490
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Administrative record header for a New York City WTC environmental file dated between May 17 and May 21, 2002.
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Technical log detailing gas chromatography mass spectrometry method parameters and calibration settings from May 2002.
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NYC-WTC_000022504
Laboratory report showing blank test results for nitrosamines and other compounds in sample AE11424 analyzed May 17-21, 2002.
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NYC-WTC_000022508
Calibration verification report listing response factors for target compounds in sample AE11424 analyzed May 17-21, 2002.
Filed in the same folder