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GCMS scan comments for sample AE11480, May 29, 2002

Machine-extracted title · confidence 100%

Laboratory commentary noting no unusual compounds detected in the GCMS scan of sample AE11480 on May 29, 2002.

NYC-WTC_000022561–000022574

Folder label: “GCMS X 5/17/12 A 5/21/02

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Scanned page image, NYC-WTC_000022571
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020521\11480.D Vial: 14 Acq On : 21 May 2002 9:12 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Benzene, 1,2,3,5-tetrachlor... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 28.90 0.21 ug/1 20576 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, l,2,3,5-tetrachloro-4,6... 242 C8H6C14 000877-09-8 37 2 7-(lhloro-4-methoxy-3-methylquino. . . 207 C11H10C1NO> 1000213-52-2 35 3 Bemzofuran-2-one, 2,3-dihydro-3,... 207 C10H9NO4 1000129-53-4 10 4 Benzenamine, 4-bromo-2-chloro- 205 C6H5BrClN 038762-41-3 9 Abundance Scan 4395 (28.902 min): 11480.D (-4388) (-) Hm/z 207.00 100.00% 207

244 5000

51 ... 63 84 104 136 180 1 28.60 28.80 29.00 29.20

niz-> 0- —H 40 60 80 100 120 140 160 180 200 220 240 m/z 244.00 54.41% Abundance #84890: Benzene, 1,2,3,5-tetrachloro-4,6-dimethyl- 207 244 5000 ' ■ i ' ■ ' ' i ‘ ■ 1 i ' ' T* 1 * 1 ! 136 28.60 28.80 29.00 29.20 m/ z 2 08.90 47.94% 51 61 75 85 99 171 0 .... Ill,, A ,,1!,,1.. 1199.121 l h 146157 1 1 1 1 II, 193 , ■ 1 । । ■ ‘** । । 1—1 । 11 229 u 4 n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #84815:7-Chloro-4-methoxy-3-methylquinoline 207 178 TI 28.60 28.80 29.00 29.20 75 5000 m/z 241.80 34.12% 41 51 63 102 115 138 164 192 119 128 0 luqlulllall—al 4lhheyaulu,4lu144——X44 89 h, । *' miz-> Abundance 40 43 60 80 100 120 140 160 180 #84704: Benzofuran-2-one, 2,3-dihydro-3,3-dimethyl-4-nitro- 77 200

207 220 240 ...... 11....... 28.60 28.80 29.00 29.20 m/z 63.20 33.14% 63 136 5000

!3 149

m/z—> oM 40 AJul 60 t80 100 120 140 al162,,179 160 180 192 iji 200 220 240 28.60 28.80 29.00 29.20

11480.D SCAN020521.M Fri May 24 09:32:16 2002 Page 7

NYC-WTC_000022571

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NYC-WTC_000022571Source: NYC Law Department, mirrored locally

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