GCMS scan comments for sample AE11480, May 29, 2002

NYC 9/11 Public Portal Document LlDrary search Compound Report

Data File : C:\MSDCHEM\l\DATA\020521\11480.D Vial: 14 Acq On : 21 May 2002 9:12 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 2-Propenal, 3-(3,4-dimethox... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.10 0.25 ug/1 24827 Phenanthrene- dl 0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 58 2 Anthracene, l-methyl- 192 C15H12 000610-48-0 42 3 cis-2-Methyl-4-phenylthiane 192 C12H16S 076097-69-3 38 4 Phenant hr ene, 9 - me t hyl - 192 C15H12 000883-20-5 38 Abundance / Scan 4769 (31.099 min): 11480.D (-4759) (-) m/z 192.10 100.00% 192

5000

82 146 96 30.80 31.00 31.20 31.40 46 120 160 Of mmIH HHmmmmmpmlt, m/z 82.00 20.54% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161

5000- ............... 1 i ' ' 1 ‘ i ’ ■ 30.80 31.00 31.20 31.40 77 121 149 177 m/z 191.00 20.26% 91 103 52 64 138 ...

m/z-> 0 mpn 1 Tp 10 20 30 40 50 60 70 80 90 100110120130140150160 170180190200 LXu Abundance #125854: Anthracene, 1-methyl- 192 • ■ i ■ ■ ■ ■ । ’ ■ i 1 ' 1 1 i 1 1 30.80 31.00 31.20 31.40 5000 m/z 146.10 17.33%

82 94 165

n/z-> 18 27 39 51 63 I h 115 126 139 150 1 176 4 „ 0+ I | I I I I | । । l‘l | 1 । I l’| 1 1 1 1 |'l 1 I I |'l I J I | । I’M I 11'1*1 1 I I IT I I j I'l'l'i 1 ] 1 1 ! 1 । 1 1 ri'] 1 । I rPi 1 I |'rl I I | 1 rli | 1 1 II 10 20 30 40 50 60 70 80 90 100110120130140150160 170180190200 Abundance #80922: cis-2-Methyl-4-phenylthiane 192 30.80 31.00 31.20 31.40 m/z 193.20 14.59% 131 5000 91 117 143 104 163 51 61 77 177 --4lHll,44l4444HHH m 0 11 H 111 ii 111 n 111 1111 l III 111 i ■ rr 11 ryr , 11 mr rrn । i'I'iT|'i . A m 1111 i'i 11 r.i m 1111 * * j 1 ' ■ > । 1 i ■ ■ 1 • i 1 ‘ n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 30,80 31,00 31.20 31,40

11480.D SCAN020521.M Fri May 24 09:32:17 2002 Page 8

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