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GCMS results sample AE08258, April 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08258 showing surrogate recovery and unknown compounds from April 2002.

NYC-WTC_000047926–000047950

Folder label: “GCMS X 4/8/02 A 4/17/02

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Scanned page image, NYC-WTC_000047947
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08258.D Vial: 16 Acq On 17 Apr 2002 9:50 pm Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 2-Propenal, 3-(3,4-dimethox... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.32 ug/L 510160 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 40 3 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 40 4 Phenanthrene, 3-methyl-______________ 192 C15H12 000832-71-3 40 Abundance Scan 3330 (22 645 min). 08258.D (-3320) (-) m/z 192.10 100.00% 192 I 5000

96 146 160 22.40 22.60 22.80 23 00 42 70 82 Qi 11" '1 r ' " 111 " r ' " I " 11 —+++ |ihI .......I'"118 I I m/z 191.10 19.10% 1— 1............. . Tn " I n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953 2-Propenal. 3-(3,4-dimethoxyphenyl)- 192 161 ... ................ 5000 22 40 22 60 22 80 23 00 77 m/z 193.10 18.92% 52 64 91 103 121 138 149 177

n/z-> Qi ...... .... 'I'...lajmns pt.. ill. 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I ‘'1 I 4 Abundance #125844 Anthracene. 2-methyH- 192 ----- 22.40 22.60 22.80 23.00 5000 m/z 146.10 14.46%

96 165 63 7—4.4831, || 115 139 150 I 176 4-rryrr nz-s 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125842 Phenanthrene, 2-methyl- ....... A, , ... 192 22.40 22.60 22.80 23.00 m/z 96.10 12.78%

5000

96

Tl/Z“> 0 27 11 ■■ ■11" 39 51 — L i" " i" " i 63115 126 139 152 185 176 74 82 ■ 'i ■ri 1 r1'1 ■'■'■"I"" I" "'I ""I'"" l''"'l "■'■'l'"''I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1 ■ I" TIT ■ i ' 22 40 22 60 22 80 23.00 ■

08258.D 041702SCAN.M Thu Apr 18 09:37:44 2002 Page 18

NYC-WTC_000047947

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NYC-WTC_000047947Source: NYC Law Department, mirrored locally

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