GCMS results sample AE08258, April 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08258.D Vial: 16 Acq On : 17 Apr 2002 9:50 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 Cyclopentasiloxane, decamet... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

12.46 0.76 ug/L 1100840 Napthalene-d8 13.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 80 3 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 40 4 N-(Trifluoracetyl)-0,0',O''-tris... 495 C20H36F3NO4Si3 054135-51-2 37 Abundance Scan 1596 (12 457 min): 08258 D (-1588) (-) m/z 73.10 100.00% 73

5000 267 355 ■ 1 1 ■ i ■ ' 1 1 r1 FTi ■ ■ । ■ ■ r1 1 '■

n/z-> 0 mm 45 108 133 154 177193 223 251 | I, 323339 uwleayalalyrufpovdugun n1' rr 111 *i ।''' 11 "r 11 ■ r> ■ j-11 TTITTTTTTTTTTT rl. i " " i" ■ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 12.20 12.40 12 60 12 80 m/z 267.00 35.73% Abundance #115273 Cyclopentasiloxane, decamethyH- 73

5000 267 ................../ \............. 12 20 12 40 12 60 12.80 355 m/z 355.10 29.40% 45

n/z-> 20 0 Ua 96 115 133149165 , 193 223 251 . “Imummupmaer 1 " ■ ■ r ■' 307323339" '*i ’' i " " i1" 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115315 Cyclopentasiloxane, decamethyl- 73 ........... H ' ' 1 1 1 1 r ' 1 1 1 1 TdT 355 12.20 12.40 12.60 12.80 267 5000 m/z 356.00 11.54%

45 323339 | ovTPmmmTTPTT191207223 251 r’t. "'I1''.. "rijt TIPTWTTTPTTTTT n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115313: Phenethylamine, N-methyl- beta..3.4-tris(trimethy . 73 12.20 1240 12.60 12.80 m/z 268.00 11.45%

5000 355

44

Tl/Z—> 0 TIT 20 40 rtherHpatr 93.. 130 147... 193 220 237 267 294310 L TIT384 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 ' . ..... M 1 ■ i 1 ■ 12 20 12.40 12 60 12 80

08258.D 041702SCAN.M Thu Apr 18 09:37:44 2002 Page 17

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