GCMS analysis results, Sample AE08267, April 22, 2002

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GCMS analysis report for sample AE08267 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048421–000048435

Folder label: “GCMS X 4/9/02 A 4/17/02”

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Data File : C:\MSDCHEM\1\DATA\020417\08267.D Vial: 24 Acq On : 18 Apr 2002 4:22 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 12.46 0.36 ug/L 557525 Napthalene-d8 13.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 87 3 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 38 4 Benzeneethanamine, N-[ (pentaf luo . . . 563 C24H34F5NO3S13 055429-13-5 37 Abundance Scan 1596 (12.457 min): 08267.D (-1582) (-) m/ z 73.10 100.00% 73

5000 267 355 ____ _______ ' ' I '■1 ' ' I ' 1 ' ' I ' ' 45 12.20 12 40 12.60 12 80 mm 108125 154 177193 251 | 323339 m/z 267.00 0 Ifuty—novyuud"gvmMunfip M 11 pi1 > i* ] । iilr 111111111 '11r " 1 T" 1 ''r " ’T I’Tt L 35.36% tVz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 267 5000 12.20 12.40 12.60 12.80 m/z 355.10 30.04% 45 191207223।।251 323339 [ 0 mmmTmmmPWTT ■ • i •'7' i " ■ . .'V. । z ''' 11..' I'' l','1' Tnn 11111 • > '- n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115273: Cyclopentasiloxane, decamethy 73

12.20 12.40 12.60 12.80 5000 267 m/z 268.00 9.84% 355

n/z-> 0 „28.14 TInupmumm 45 l 96 115 133149165 , 193 223 251 307323339 • ■ r '" i "i1 " 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 11"r1

Abundance #115313: Phenethylamine. N-methyl- beta ,3.4-tns(trimethy . 73 12.20 1240 12 60 12.80 m/z 356.10 9.62% 5000 355

44 l ... , 1 93 130147 193 220 237 267 294310 _ 384 0 ' I'11' T ' T'1 “l1 H ' 1111111 ''''' I''''' 11 ''11 '1'1 r '1' 11'' rl111 1 l r 1 ■ prr >h-| i r| i) r''' । > i' ।''' ,...... M, .......... Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 12.20 12.40 12.60 12.80

08267.D 041702SCAN.M Thu Apr 18 10:01:02 2002 Page 6

NYC-WTC_000048430

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