GCMS results sample AE08254, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08254.D Vial: 12 Acq On : 17 Apr 2002 6:32 pm Operator: Nefliu Sample : sample Inst : Instrumen MisC : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

12.46 0.53 ug/L 800650 Napthalene-d8 13.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 3 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 43 4 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 38 Abundance Scan 1596 (12 457 min) 08254 D (-1590) (-) m/ z 73.10 100.00% 73

5000 267 355

45 12 20 1240 12.60 12.80 125 154 193 223 d 323 0- n-r-r TTT m/z 267.00 37.30% n/z- > 50 100 150 200 250 300 350 400 450 500 550 it Abundance #115315: Cyclopentasiloxane, decamethyl- 73

5000 267 355 . . n... 12 20 12 40 12.60 12 80 m/z 355.10 30.42% 45 207 323 1..................... Tl/z—> 01 50 100 150 ' Pifrr ' 1a ' 200 250 300 350 400 450 500 550 Abundance #115273: Cyclopentasiloxane, decamethy- 73 —=p= ............. 12 20 12 40 12.60 12 80 5000 267 m/z 268.00 11.27% 355 45 193 223 0—r ,‘ ’Ji , 103 133 1650,440 .1 293 323 i 1 1 Tl/Z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115316: Benzeneethanamine, N-[(pentafluorophenyl)methylen. . 73 355 12 20 12.40 12.60 12.80 m/z 356.00 10.84% 5000

Tl/Z-> 0- —4 45

50 1 117 147 179 207 251 281 " । 1 r.’. t r r'1 { ' 100 150 200 250 300 386 429 458 i ■ ■ ■ ' i ■ > ■ ■ i • • 350 400 1-1" i ’ r 1 'i 1 1 450 500 548 550 .. n 12.20 12 40 TBT 12 60 12.80

08254 .D 041702SCAN.M Thu Apr 18 09:23:29 2002 Page 7

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