GCMS surrogate recovery results, April 22 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08260.D Vial : 17 Acq On : 17 Apr 2002 10:40 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Cyclopentasiloxane, decamet... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

12.46 0.39 ug/L 569968 Napthalene-d8 13.49

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 72 3 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 37 4 Benzoic acid, 2-[(trimethylsilyl... 282 C13H2203Si2 003789-85-3 32 Abundance Scan 1596 (12 457 min): 08260.D (-1585) (-) m/z 73.10 100.00% 73

5000

40 103 154 193 223 , 267

323 355 . .... n TIT i 1 ' 12 20 12.40 12.60 12.80 0- - r............ I1 i 1 । |l । m/z 267.00 31.22% n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 267 5000 12 20 12.40 12.60 12.80 m/z 355.00 27.59% 45 207 :323 [................. 0t—r • ■ । । । ' n/z—> 50 100 150 200 250 3001 ' 350 ' 400 ' 450 500 ' 550 Abundance #115273 Cyclopentasiloxane, decamethyl- 73

12 20 12 40 12.60 12.80 5000 267 m/z 356.00 11.77% 355 45J | | 103 1 33 1 65 102 193 223 . 293 323 I 0+ ' 300 ' 350 ' ' 400 ' ' 450 ' 500 ' 550 /z-> 50 100 150 200 250 Abundance #115316. Benzeneethanamine, N-[(pentafluorophenyl)methylen . it............................... 73 355 12 20 12.40 12.60 12.80 m/z 268.00 10.11%

5000

45 —। 117 147 179 207 251 281 386 429 4 58 548 0 ------ TTITTT n/z- > 50 100 150 200 250 300 350 400 450 500 550 12 20 1240 12.60 12.80

08260 .D 041702SCAN.M Thu Apr 18 09:45:55 2002 Page 12

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