GCMS Analysis Results, Sample AE08261, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08261 .D Vial: 18 Acq On : 17 Apr 2002 11:29 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Cyclopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

12.46 1.75 ug/L 2959100 Napthalene-d8 13.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 87 3 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 47 4 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 37 Abundance Scan 1596 (12.457 min): 08261 D (-1588) (-) m/ z 73.10 100.008D 73

5000 267 355 /I 45 12.20 12.40 12.60 12.80 0- 108 - -154 193 237 Aorm* re t 323. m/z 267.00 36.61% n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 267 ....... 5000 12 20 1240 12.60 12.80 m/z 355.00 30.27% 45 207 323 1 0- i , ----- n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115273 Cyclopentasiloxane, decamethy- 73 I \ 12.20 12.40 12 60 12 80 5000 267 m/z 356.10 11.28% 355 45 103 133 165 193 223 . ;293 323 1 ol ,, 1 1, -PTHr /z— > 50 100 150 200 250 300 350 400 450 500 550 Abundance #115316 Benzeneethanamine, N-[(pentafluorophenyl)methylen ........................... 73 355 12 20 12 40 12 60 12.80 m/z 268.00 10.42% 5000

45 — । H7 147 179 207 251 281 I 386 429 458 548 0- ------- M /z-> 50 100 150 200 250 300 350 400 450 500 550 12.20 12.40 12.60 12 80

08261.D 041702SCAN.M Thu Apr 18 09:47:23 2002 Page 11

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