GCMS Analysis Results, Sample AE08261, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08261.D Vial: 18 Acq On : 17 Apr 2002 11:29 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 5 2-Propanone, 1,1,1-trichloro- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.04 0.77 ug/L 969889 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 47 2 Hexane, 2-methyl- 100 C7H16 000591-76-4 9 3 1-Propanamine 59 C3H9N 000107-10-8 9 4 4-Penten-2-one____________________ 84 C5H80 013891-87-7 9 Abundance Scan 503 (6 035 mm)' 08261 D (-498) (-) m/z 43.05 100.00% 43 A 5000

49 59 1 83 181 -1-17 125 .. N.... 5.60 5.80 6.00 6 20 6.40

n/z-> ol ■ ■ ।'' ■ ■ । 10 20 '1 ■ ।' 30 3744 40 । Per 1 • * । |'''' । 1 । । ' । । । I I1 > ' । । > । I—mmmmmpa** -i 111 । ■ 1 । 50 60 70 80 90 100 110 120 130 m/z 59.10 18.85%

Abundance #3877 2-Propanone, 1,1,1-trichloro- 43

5000 _- 5.60 5.80 6 00 6.20 6.40 m/z 58.00 10.14% 15 I 27 36 49 55 63 76 83 91 97 hq 117 125 1 01 —1 +1Imp Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #109388: Hexane, 2-methyl- 43 ................... 5 6 0 5 8 0 6.00 6.20 6.40 5000 m/z 101.10 7.51% 29 57 85 — 51 71 100 01 Tr-r-p-r t-ndi ' i 11 111'1 11 1 i1 111 n/z-> 10 20 30 40 50 60 70 80 !90 100 110 120 130 Abundance #108234 1-Propanamine 3b 5 60 5 80 600 6 20 6.40 m/z 124.90 6.28% 5000

59 41

n/z- > 0- pip 10 20 30 l 47 53 , 1114 40 I ' ' 1 11 50 60 70 80 90 100 110 120 130 5 60 5 80 6 00 6 20 6.40

08261.D 041702SCAN.M Thu Apr 18 09:47:22 2002 Page 10

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