GCMS analysis results for sample AE08064, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020415\08064 .D Vial: 21 Acq On 16 Apr 2002 3:10 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 2-Propanone, 1,1,1-trichloro- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

6.04 0.50 ug/L 428273 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 45 2 Butane, 2,2,3,3 - tetranitro- 238 C4H6N4O8 020919-97-5 16 3 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 12 4 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 Abundance Scan 503 (6.035 m;n) 08064 D (-497) (-) m/z 43.25 100.00% 43 4 5000

1** TT r 125 5.60 5.80 6.00 6 20 6 40 01 37 49 1 1 1 ' 1 1 1 1 ' ' 'T' ,,'l, f 14 ' 144 . Hh* 61 । 83 i | > ' J.'| . ... । i 97 119.1. m/z 125.20 11.08% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3877 2-Propanone. 1.1,1-trichloro- 43

5000 5 60 5 80 6 00 6 20 6.40 m/z 83.20 6.84% 13 | 27 36 49 55 63 76 83 91 97 110 117 125 ol ' I ' i1" i ' MIt ' 11 1 ’’i ■ ■ ■ 1 I1'' ■ ' i ' ' 1 ■ i 1 1 r' i ' ' ’’i । । .'.'i . . । . n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3995 Butane, 2,2,3,3-tetranitro- 30 43 ... n 5.60 5.80 6.00 6.20 6.40 5000' m/z 127.10 6.78%

15 53 I Tl/Z—> 01 —H 10 20 30 37 # +4——— 40 50 —1 60 69 70 80 86 90 100 110 120 130 1 ''i ■ ' 1 ■ i ■ ' 1 ' i 1 ' ' ' i ' ■ ■ ■ i ' ' 1 1 i 1 1 ' 1 i 1 '

Abundance #3861: 2-Propanone. 1,1-dichloro- 43 5.60 5 80 6 00 6.20 6.40 m/z 97.20 6.25%

5000

15 27 I 49 55 63 I 36 +1PTTT 76 83 93 125 0 —19+ —hr i1111 I' ' 1 ■ i ' ■ ■ ■ i ' 1 ■ ' i 1 ' 1 1 I ' 1 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5 60 5.80 6 00 6.20 6 40

08064 .D 041202SCAN.M Tue Apr 16 13:53:51 2002 Page 7

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