GCMS analysis results for sample AE08064, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08064.D Vial: 21 Acq On : 16 Apr 2002 3:10 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 3 3-Pentanol, 3-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.97 0.33 ug/L 281383 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 Acetic acid, 3-[1,3]dioxolan-2-y. .. 174 C8H1404 1000186-02-3 28 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 3-Pentanol, 3-methyl-_______________ 102 C6H140 000077-74-7 9 Abundance Scan 492 (5 970 min) 08064 D (-486) (-) m/z 73.30 100.00% 73

5000

0'1111"111' 43

_ _____ H ' i' " ' i' 87 ’ i '1''' i " ■ ■ i' ■ ■ ■ r ■ ■' r ' ■ • r '111 '''' I '1' ■ i ‘1 ■ ■ r ' ■ ■ r ■ ' i ■ ■ ■ ■ i ■ 1 5.60 m/z 5 80 43.30 1 6 00 6.20 28.37% 6.40

n/z—> 10 20 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #114875 3-Pentanol, 3-methyl- 73

5000 TIT—mr 5 60 5 80 6 00 6.20 6 40 . 45 55 m/ z 41.30 12.42% 15 2, 37 1/ 637 0- 111. ■< t rr 14pr T‘‘0T‘‘‘1UUTTUTTTTT , 63 i । 87 । ■ ■ ■ ■) ■ ■ • ■ । > ■ i ■ i1'11 ■ ■ ■ • । ■ ■ ■ ■ । ■ > ■ • । > ■ ■ ■ j ■ ■ 111 ■ -1 ■ । ।

Tl/Z~> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance

I #25344 Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 6.40 5000- m/z 45.30 10.65% 43 27 55 , 87 113 131 174 0- .......... 1 .... ‘I‛I‛1 ■ 11 l’’ 'T' I ' ■ | 1 ■ !'l | • ' • • | ■ r ' ' | | ■ ■ • . | > 1 | • ' 1 ' | ■ > > ■ | ■ ■ ■ ' | ■ > ■ • | > ' n/z— > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #857 N-Ethylformamide 3b 5 60 5 80 6 00 6 20 6.40 73 m/ z 40.20 7.80% 5000 44 58

18 0 - — r " ' i''1" i ■ ■ " i11 ■' i11' ■ i" ■ ■ i ■1 ■ ■ i' ■1' r " ' i " " i11 ■' i1 " ' i " n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20 6 40

08064.D 041202SCAN.M Tue Apr 16 13:53:51 2002 Page 6

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