GCMS results sample AE08258, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08258.D Vial: 16 Acq On : 17 Apr 2002 9:50 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 3-Pentanol, 3-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.97 0.79 ug/L 865749 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 2 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 36 3 Acetic acid, 3 -[1,3]dioxolan-2-y. . . 174 C8H14O4 1000186-02-3 33 4 1-Propene-1-thiol 74 C3H6S 000925-89-3 23 Abundance Scan 491 (5.964 min): 08258.D (-487) (-) m/z 73.10 100.00% 73

5000- 43 5.60 5.80 600 6.20 6 40

n/z-> 10 O-mpp 20 30 40 L 50 60 70 87 "' ■ । 11 80 103 ।1 " ' r'1 " i " '11" 1 11'1'11 " " i " " r 1 " i " ■ ■ i11 90 100 110 120 130 140 150 160 170 180 m/ z 43.10 29.87% Abundance #114875 3-Pentanol. 3-methyl- 73

5000- 1**)4* 11 5.60 5.80 6 00 6 20 6.40 45 55 m/ z 41.10 11.32% 27 7 87 15 71 +63— I 01 ' i 1 ''' 11' '1 'T1'1 '| I 'I i 1TTTTT ■ I ‘'111'1' I " ' ' 11' Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25351 Butane, 2-methoxy-2-methyl- 73 A kah /044 Ah AAA, 41A4AAA 5 60 5.80 6 00 6.20 6.40 5000 m/ z 45.10 10.68%

29 43 55 87 A n/z-> ol -pat...... mp 10 20 PIHPTTTTTWITTT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25344 Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5 60 5 80 6 00 6.20 6 40 m/ z 40.00 7.49% RNYwyAWW 5000-

43 55 . 87 27 113 131 174 0 TIT mPmm TTWTuuPOPur /z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5 60 5 80 ' 6.00 6.20 6.40

08258.D 041702SCAN.M Thu Apr 18 09:37:42 2002 Page 8

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