GCMS blank analysis results for sample AE08251, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\0408LB.D Vial: 3 Acq On 17 Apr 2002 11:01 am Operator: Nefliu Sample 04/08 1b Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.97 0.32 ug/L 307363 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 25 2 Acetic acid, 3-[1,3]dioxolan-2-y. . . 174 C8H14O4 1000186-02-3 23 3 Pentane, 3 -methoxy- 102 C6H140 036839-67-5 12 4 Pentanol, 5-amino­ 103 C5H13NO 002508-29-4 9 Abundance Scan 493 (5 976 min) 0408LB.D (-486) (-) m/z 73.10 100.00% 73

5000 43

87 103 5 60 5 80 6 00 6 20 6 40 01 ' I 1 'TT^ TOmuuUugu m/z 43.10 2 4.23% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #114875 3-Pentanol, 3-methyl- 73

5000 Ai A M A A A AA J A AAMMMM, MA 5.60 ' 5.80 ' 6.00 6.20 6.40 . 45 55 m/ z 40.00 15.02% 27 87

Tl/Z--> 0+ 15 .. 1,1 ■ i ■ ■■'

10 11111 'l :20 +371,763..,, 30 40 63 , 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25344: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 i 1 1 1 ' i ■ ■ 5.60 5.80 6.00 6.20 6.40 5000 m/ z 45.10 13.24% 43 2755 . , 87 113 131 174 0 ■ i " " i' TTT " " i " 1,11' ‘ ■ i ■ " 11 " i" ' ■ I ■ " 11 " " i " 11111" I ■1 ■ ■ i1 ■ | Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25472: Pentane, 3-methoxy- 73 5 60 5 80 6 00 6 20 6 40 m/ z 41.10 12.21% 5000 45

/z-> 0 TTT 10 20 29 30 40 , 5 EE 50 60 70 80 101 1 • I ■ ■ ■' 11'111 ■1 >' 111 ■ 11 ■ ■111 ■' ■ ■ 1111»I ■ ■ ■111 ■ ■ ■ l ■ • 90 100 110 120 130 140 150 160 170 180 AAAAAAAMAILL 5.60 5 80 6.00 6 20 6 40

0408LB.D 041702SCAN.M Thu Apr 18 09:09:39 2002 Page 5

NYC-WTC_000047764