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GCMS analysis results for sample AE08253, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08253 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047830–000047850

Folder label: “GCMS X 4/8/02 A 4/17/02

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Scanned page image, NYC-WTC_000047841
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08253.D Vial: 11 Acq On 17 Apr 2002 5:42 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 3-Pentanol, 3-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.97 0.30 ug/L 325050 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 2 Acetic acid, 3- [1,3]dioxolan-2-y . .. 174 C8H14O4 1000186-02-3 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 5 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 4 Abundance Scan 493 (5.976 min): 08253.D (-479) (-) m/ z 73.10 100.00% 73

5000 43 i j r~r~r~r~j iiii । rm n l i i-1 । i 1

i 1 55 87 5.60 5.80 6.00 6.20 6.40 01 " i" " i 1 . i |‘n q . i1!1.1! . . i 1 I Div r i \ | i I I I । I I I f | i | | | | r I I I | I I I I | I i I I | i i I I | rrr j I I I I | I I m/z 43.05 25.89% /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #114870: 3-Pentanol, 3-methyl- 73

5000 55 5.60 .l .. 1 I ' ' 1 5.80 6.00 I 1 1 1 1 II .>11 6.20 6.40 43 m/ z 45.10 12.31% 29 | 87 .......ml lr I I I I I i : । . I1. I । . > . । । । । i > । . । । । । i ."I q | | I q | I | | | I . . I | I . I | | I | o1 > l | < > I > I r-t r l | < > . 11′11 ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25344: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 I I I I I I I I I I I 1 ] I- 5.60 5.80 6.00 6.20 6.40 5000 m/ z 41.10 9.01% 43 27 0 I I I I > ! < I I I I I [ I I I 111T 55 -Tpm ,i TTT + 87 174 113 | ' 1 1 1 | 131 | 1 ■ 1 1 | 1 ' 111' ’11 * < • < I m/z-> Abundance 10 20 30 40 50 60 70

33 80 90 100 110 120 130 140 150 160 170 180 #857: N-Ethylformamide 5.60 5.80 6.00 —LAA 6.20 6.40 73 m/z 71.00 7.28% 5000 44 58 I 18 0 - II | । i i i |'i I । I [ I । i i । i । । । । । । । । । I i > i । r i I >‘| | I I l | 1 vr]” I I I [ r I T I | I I | I j I I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 600 6.20 6.40

08253.D 041702SCAN.M Fri Apr 19 08:38:00 2002 Page 8

NYC-WTC_000047841

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NYC-WTC_000047841Source: NYC Law Department, mirrored locally

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