GCMS analysis results, Sample AE08264, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08264.D Vial : 21 Acq On : 18 Apr 2002 1:56 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 3-Pentanol, 3-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.97 0.42 ug/L 504056 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 2 Silane, tetramethyl- 88 C4H12Si ' 000075-76-3 28 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 28 4 N-Ethylformamide 73 C3H7NO 000627-45-2 9 Abundance Scan 491 (5.964 min): 08264.D (-485) (-) m/z 73.10 100.00% 73

5000 43 5 60 5.80 6 00 6 20 6 40 0- ....................... 49. ........... . 87 103 i ■ ■ i ■ ■•i'i । । । । । . m/z 43.05 28.21% n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 Abundance #114875: 3-Pentanol, 3-methy- 73

5000 .............. N, . ........... . 5 60 5.80 6 00 6.20 6 40 55 m/z 45.10 11.17% 45 87 01 ...... 15.2132.391,1,1,50 T 67— 1 1 I 1 1 1 ' I ' ' ' 1 I I ' 1 1 I ' ' ' 1 r1 1 ' ' I I ■ ■ । ■ 1*' 1 i 1 1 1 * i 1 ■ ' r i ■ n/z- > 0 10 20 30 40 50 60 70 80 90 100 110 Abundance #114826' Silane, tetramethy- 73 __ ----- 5 60 5.80 6 00 6.20 6 40 5000 m/z 41.05 10.66%

43 15 0- 2 । । I । 24 29,35 ,48 5359 65 ' I /PP———mTt 1, 79 88 ' i ■ ■ ■ 1 i ■ ■ ■ ■ i 1 1 1 ' i ■ ' 0 ' 10 n/z-> Abundance 20 30 40 50 60 #25349: Silane, tetramethyl- 70 80 90 100 110 ahqanZuhaansal“annuka 73 5.60 5.80 6.00 6 20 6.40 m/z 71.00 7.22%

5000

29 43 2 15 ,i , 38 48 55 60 66 |, 79 88 0 । । । । । i-r-| . i'i । । । । ili’a . . . 11 in 1 । . i'| ■ . . . |-t I ■ > । ■ i । ■ • ■ ■ । । ■ i ■ /z- > 0 10 20 30 40 50 60 70 80 90 100 110 5.60 5.80 6.00 6.20 6.40

08264.D 041702SCAN.M Thu Apr 18 09:52:45 2002 Page 12

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