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GCMS analysis results, Sample AE08264, April 22, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08264 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048355–000048377

Folder label: “GCMS X 4/9/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08264.D Vial: 21 Acq On : 18 Apr 2002 1:56 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Hexanal Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.14 0.42 ug/L 499859 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanal 100 C6H120 000066-25-1 46 2 Hexanal 100 C6H120 000066-25-1 46 3 Hexanal 100 C6H120 000066-25-1 43 4 Hexanal 100 C6H120 000066-25-1 43 Abundance Scan 351 (5 142 min): 08264.D (-344) (-) m/z 56.10 100.00% 44 56 129 5000

72 82 ' 1 I ' 1 ' ' I 1 ' ' ' I ' ' 1 1 I * ' ' ’ 1 1 208 4.80 5 00 5 20 5.40______ 0+ ' ' i I ....III1 1 Iil1 ' 1911 1 ........... | i, Il 11|TT 1 1 1 1 1 ' I . ........ . - m/z 44.10 98.86% Tl/Z-> 20 40 60 80 100 120 140 160 180 200 Abundance #110562: Hexanal 44 56

5000 “PrYY ■ ■ i 1 27 4 80 5 00 5.20 5.40 72 82 m/ z 41.05 79.85% 15 n/z— > 01 T 20 —T 40 14 60 j 80 | 100 100 120 140 160 180 200 Abundance #110561. Hexanal 44 56 MMM. 4.80 5.00 5 20 5.40 5000 27 m/z 128.90 66.61%

72 82 0+ ■ 1 i ' 4— 1 1 । | 98 n/z--> 20 40 60 80 100 120 140 160 180 200 Abundance #10785: Hexanal W.............. 44 , 4.80 5 00 5 20 5.40______ 56 m/z 45.00 56.53% 5000 29 72 82

ti/z--> 0 — 20 40 u ' 1 I 60 । | 80 100 100 120 140 160 180 200 M.............. 4 80 5 00 ,0540... .. 5.20

08264.D 041702SCAN.M Thu Apr 18 09:52:45 2002 Page 11

NYC-WTC_000048369

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NYC-WTC_000048369Source: NYC Law Department, mirrored locally

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