GCMS surrogate recovery results, April 22 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08260.D Vial: 17 Acq On : 17 Apr 2002 10:40 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L ********************************************************************* Peak Number 4 Hexanal Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.14 0.32 ug/L 351719 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexanal 100 C6H120 000066-25-1 50 2 Hexanal 100 C6H120 000066-25-1 49 3 Hexanal 100 C6H120 000066-25-1 47 4 Hexanal 100 C6H120 000066-25-1 47 Abundance Scan 350 (5.136 min). 08260.D (-346) (-) m/z 44.05 100.00% 44 56

129 5000

72 82 208 4 80 5 00 5.20 5.40 0+ L’ ulii I ill ll 191 r 1 1 I 1 . ...... 1’ 1 1 F-— -4— ....200 m/z 56.05 91.55% n/z-> 20 401 60 80 100 120 140 160 180 Abundance #110562: Hexanal 41 , 56

5000 TI 27 4.80 5 00 5 20 540 72 82 m/ z 41.10 88.41%

n/z-> Abundance 0+ . 1520 . '•40I 41 „ 1 60 80 100 100 120 #10785: Hexanal 140 160 180 200 A . 56 4 80 5 00 5.20 5.40 5000 m/z 45.10 69.52% 29 72 82

n/z-> 0+ —l 20 40 |_ L । | 60 80 100 100 120 140 160 180 200 Abundance #110563 Hexanal A,,.... . 41 4 80 5 00 5 20 5 40 56 m/z 43.10 68.10% 27 5000

72 82

n/z-> 0 ■ ■ i 20 > ■ ■ ■ । 40 14 60 80 100 120 140 160 180 200 11 I ' 1 1 1 I r' 1 ' I ' ' 1 ' I ■ ' ' 'I 4.80 5.00 5.20 5.40

08260 .D 041702SCAN.M Thu Apr 18 09:45:52 2002 Page 9

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