GCMS analysis results, Sample AE08266, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08266.D Vial: 23 Acq On : 18 Apr 2002 3:33 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L Peak Number 3 Hexanal Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 5.15 0.28 ug/L 335555 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexanal 100 C6H120 000066-25-1 43 2 Hexanal 100 C6H120 000066-25-1 37 3 Hexanal 100 C6H120 000066-25-1 37 4 Hexanal ______________________ 100 C6H120 000066-25-1 37 Abundance Scan 352 (5.148 min): 08266 D (-347) (-) m/z 56.10 100.00% 55 44

129 5000- ... ... 72 82 4.80 5.00 5.20 3& 50 540

Tl/Z-> 0+ ' ' I ' 1 ' 1 I ' 1 1 1 I 1 1 I I 10 20 30 40 III50 II l 1 ' 1 1 1 60 70 80 90 ' ' I ' ■11 ■''1 r"’’111... .. .. .. .. .. ........ ............. 100 110 120 130 m/z 44.05 /i 78.87% Abundance #110562: Hexanal 44 56

5000 A . 27 4 80 5.00 ' 5.20 ' 5.40 '' 72 m/z 45.10 71.91% 82

n/z-> ol ' ■ i ' 15 10 ''■ 1 i ■ 20 I 30 38 I 40 +50,1 50 45 80| 90 100 100 60 ' 1 Ili 1 I I1 ' v* l ’ 1*1***’) 110 120 130 70 Abundance #110563 Hexanal 41 56 i | ’ I ■ ■ ' ■ I • 4 80 500 5.20 5.40 27 5000 m/z 41.10 71.76%

72’ 82

■n/z-> . I 37 0+ —TPPPTT 10 20 30 40 150. 50 — — 60 70 80 90 100 110 120 130 Abundance 44 #10785: Hexanal MMMMM Hnnkw 56 4 80 5.00 5 20 5.40______ m/ z 57.10 53.77% 5000 l 29 72

n/z-> 0 ........ 10 20 Il30l,. 3440 +50.11651414 50 60 70 80 90 94 100 r 1'1 i1 100 110 1 i ■ ' 1 • i ■ ■ ■ 1 i 120 130 5.20 1. 5.40 TT

08266.D 041702SCAN.M Thu Apr 18 09:59:56 2002 Page 8

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