GCMS analysis results, Sample AE08266, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08266.D Vial: 23 Acq On : 18 Apr 2002 3:33 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Acetonitrile, dichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 3.67 0.41 ug/L 485665 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 3 Allyl mercaptan 74 C3H6S 000870-23-5 32 4 Thiirane, methyl- 74 C3H6S 001072-43-1 5 Abundance Scan 100 (3.667 min): 08266 D (-94) (-) m/ z 74.00 100.00% 74

82 5000 47 A 38 3.40 3.60 3.80 4 00

n/z- > 0+ -- 10 20 30 40 50 60 70 80 I TIB 8890—..100m P110H m/z 81.90 51.62% Abundance #28338: Acetonitrile, dichloro- 74

5000 82 A 3.40 ' 3.60 ' 3.80 4.00 47 m/z 76.00' 33.43% 35 12 0+ -r-r-j-t-r-r-r-j- .26,1,49.10 62......... । ■ i 1 ■ । ■ i ■ , 108 ' ' i ' ' ' ' i ' ■ ' ' I ' 1 ' ' i n/z- > 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342 Acetonitrile, dichloro- 74 35 1................ ...... 3.40 3.60 3.80 4.00 5000 82 m/ z 83.95 29.39%

ol 1 ■ i ■ ' 1 1 i ■ ■ ■ ■ i 40 — 47

■ । ' 1 1 । ' TIl 1 ■ i ' ■ ■ 1 i ' ■ ■ ■ i ■ 1 Mwka/wnp Wo n/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28161 Allyl mercaptan 4n 74 340 3.60 3.80 4 00 m/z 47.00 25.50% 5000

47 wJh n/z- > 0 - 10 20 27 33 I 30 40 JlU 50 3-^60 .. 99,1 70 80 90 100 110 340 3.60 3.80 4.00

08266.D 041702SCAN.M Thu Apr 18 09:59:56 2002 Page 7

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