GCMS analysis results, Sample AE08266, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08266.D Vial: 23 Acq On : 18 Apr 2002 3:33 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Heptane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

3.16 0.29 ug/L 347813 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane 100 C7H16 000142-82-5 47 2 Decane, 2,5,9-trimethyl- 184 C13H28 062108-22-9 47 3 Heptane 100 C7H16 000142-82-5 38 4 1-Butanol, 2-methyl-, propanoate____ 144 C8H1602 002438-20-2 37 Abundance Scan 13 (3 156 min)' 08266.D (-4) (-) m/z 57.10 100.00% 5l7

43 5000 71 /. m , r. । । । 4 .

100 3.20 3.30 3.40 3.50 3.60 86 ।

Tl/Z-> 0- 1 1 I 1 1 1 ■ i ' ■ ' ' i ■ 0 10 20 ....Wl,.?,,! I......T 30 40 50 60 70 80 90 100 110 120 m/z43.10 62.05% Abundance #109303: Heptane 43

5000 29 57 71 3.20 3.30 3.40 3.50 3.60 m/z 56.10 37.19% 100

n/z-> 0- 15 1 । l’i । 1 1 I........... 1 0 1 10 20 +37l +5114 30 40 50 60 65 i ■ ■ ■ 70 80 'I1 77 85 | pBlysanu...... । । । । । । । 90 100 110 120 Abundance #16457: Decane. 2,5,9-trimethy- 57 3.20 3.30 340 3.50 3 60 5000 43 m/z71.10 35.79% 71

85 99 113 0- 11 " I " +- PPm n/z- > Abundance 0 10 20 30 40 50 60 70 #109598: Heptane 80— 90 100 110 120 __ 43 3.20 3.30 3.40 3.50 3 60 m/z 41.05 29.83% 5000- 57 29 71

100

Tl/Z-> 0 ......... 0 10 - ... 20 11/1137, 30 40 +5114 50 63 TIn 11* ' 1 I । 60 70 80 85 90 100 110 120 3.20 3.30 3 40 3 50 3 60

08266.D 041702SCAN.M Thu Apr 18 09:59:56 2002 Page 6

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