GCMS results sample AE08256, April 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08256.D Vial: 14 Acq On : 17 Apr 2002 8:12 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Heptane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

3.15 0.29 ug/L 337321 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane 100 C7H16 000142-82-5 53 2 Butane, 2,2-dimethyl- 86 C6H14 000075-83-2 47 3 Heptane 100 C7H16 000142-82-5 39 4 Hexane, 2,3,5-trimethyl- 128 C9H20 001069-53-0 38 Abundance Scan 13 (3 156 min): 08256.D (-3) (-) m/z 57.05 100.00% 57 43

71 5000-

100 86 3.20 3.30 3.40 3 50 3 60

n/z-> 0- 1 1 I ’ 1 1 1 1 1 ' ' ,_p 1 1 ' I ' 0 10 20 30 37 —4 111.49,0 40 50 60 70 80 90 100 110 " 43.10 83.78% Abundance #109303: Heptane 43

5000 29 57 71 3.20 3 30 3.40 3.50 3.60 m/z 71.10 53.79% 100

m/z-> 0 0 1 10 15 ' 1 I 20 134 +511Ii ' ' ' 1 30 40 50 I60 65 70 77 1 ' ■ ' i ■ 80 85 1 i ■ ’ ■ 1 |I'1 ' 1 1 l 1 90 100 110 Abundance #109563: Butane, 2,2-dimethyl- 48 57 A4A3.20 3 30 3 40 3.50 3.60 5000 m/z 41.05 52.16% 71

Tl/Z-> 01 0 I ' ' ' ' I ' 1 1 1 I ' ' ' ' I ' ' ' ' I 10 20 30 3! 40 +51 ...... |‘ 50 60 70 80 ..................... 103 , 90 100 110 Abundance #109598. Heptane 43 3.20 3.30 3.40 3.50 3.60 m/z 56.10 42.17%

5000 57 29 71

100 0 I, 38 +51 63 85 ' 1 1 1 i ■ ■ *....... I ' n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 3 20 3.30 3.40 3.50 3.60

08256.D 041702SCAN.M Thu Apr 18 09:27:12 2002 Page 6

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