GCMS results sample AE08256, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020417\08256.D Vial: 14 Acq On 17 Apr 2002 8:12 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 3-Buten-2-ol, 2-methyl­ Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 4.99 0.26 ug/L 295910 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 72 2 Butenol, methyl- 86 C5H10O 060766-00-9 50 3 Furan, tetrahydro-2-(methoxymeth... 116 C6H12O2 019354-27-9 42 4 Butane, 2-bromo-2-methyl- 150 CSHllBr 000507-36-8 42 Abundance Scan 326 (4 995 min) 08256.D (-322) (-) m/z 71.10 100.00% 43 71

5000 55 , A... . n/z-> ol -47lllu4 +—4— 10 20 30 40 50 60 70 80 90 ' I • ' ' ’ I ’ ' ' ' I 1 ' ' 1 I 1 ' ’ ' I ' 1 100 110 120 4.60 m/z 4.80 43.10 5 00 5 20 91.58% 5 40

Abundance #114556: 3-Buten-2-ol. 2-methy- 71 43

5000 —W MVP P 59 4 60 4 80 5 00 5 20 5 40 27 m/ z 41.10 55.54% 53

Tl/Z—> ol 10 —20443744 30 40 HL 50 +46544... 60 70। 80 86 ' 1 ' 1 I ' ' 1 ' I ' ' ' 1 I ' ' ' ’ I ' ' 1 ‘ I ' 1 90 100 110 120 Abundance #24435 Butenol, methyl- 43 7h wWn MhMwy/y 4.60 4.80 5 00 5 20 5 40 5000 59 m/z 69.10 40.22% 27 | 15 53 ol | I PPTP 37 । +4L +6544 11 79 86 n/z— > 10 20 30 40 50 60 70: 80 90 100 110 120 Abundance #24361 Furan, tetrahydro-2-(methoxymethyl)- 71 4.60 4 80 ' 5 00 ' 5.20 5.40 ' 43 m/z 55.10 35.98% 5000

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Tl/Z-> 0 10 15

20 43714 30 40 51 ,58 65 - 70 80 1 I'1'1 ''’'I 1 1 1 50 60 83 90 97 100 110 116 120 ................ .... ....................................... 4.60 4.80 5 00 5.20 5.40

08256.D 041702SCAN.M Thu Apr 18 09:27:13 2002 Page 7

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