GCMS analysis results for sample AE08429, May 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\08429.D Vial: 16 Acq On : 19 Apr 2002 10:54 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 3-Buten-2-ol, 2-methyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.81 ug/1 1108360 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 81 2 Butenol, methyl- 86 C5H10O 060766-00-9 53 3 3-Penten-2-ol 86 C5H10O 001569-50-2 53 4 Furan-2-carbonyl chloride, tetra... 134 C5H7C1O2 052449-98-6 50 Abundance Scan 328 (5.006 min): 08429.D (-321) (- m/z 71.1.0 100.00% 43 71

5000 55 59 ■ i 1 ■ ■ 1 I Py 39

mH +516 —, uupupuutini 4.60 4.80 5.00 5.20 5.40 75 8487 " i" ’' r ' " i" " r " 11" " 11 m/z 43.10 96.93% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #114555: 3-Buten-2-ol, 2-methyl- 71 43

5000 TTTTTTTRYP 59 4.60 4.80 5.00 5.20 5.40 27 31 39 m/z 41.20 72.17% 53 1518 " i1 r" i" " |" I ■ i H ++ 86 — . .................. ^I, '1' i ■1" I" " i1 ■" i" " i 111111111 TT m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #24435: Butenol, methyl- 43 71

4.60 4.80 5.00 5.20 5.40 5000 59 m/z 69.10 48.40% 27 15 31 39 53

/z-> 5 "r1 —14+ .18,2411—394+4 46.59,1,561, 63,674 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ,74 79 8386 11' I " " r 1 ” i11111" " i

Abundance #114531: 3-Penten-2-ol 71 4.60 4.80 5.00 5.20 5.40 43 m/ z 55.10 34.34% 5000

27 39 86 - 31 36 46 5053 58 62 67, TTPTTTTTTTTT, 111111111111 rt-1111 11111 H 11 ■^..^1............... li, n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.60 4.80 5.00 5.20 5.40

08429 .D SCAN020418 .M Thu May 02 15:37:58 2002 Page 3

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