Laboratory report documenting GCMS analysis of sample AE08431 conducted on May 6, 2002, including surrogate recovery data.
NYC-WTC_000048121–000048133Folder label: “GCMS X 4/9/02 A 4/19/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\020419\08431.D Vial: 18 Acq On : 20 Apr 2002 12:52 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e
Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1
Peak Number 2 3-Buten-2-ol, 2-methyl- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T. 5.01 0.48 ug/1 681179 1,4-Dichlorobenzene-d4 11.38 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 87 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 80 3 Butenol, methyl- 86 C5H10O 060766-00-9 64 4 3-Methoxybut-l-ene 86 C5H10O 017351-24-5 45 Abundance Scan 328 (5.006 min): 08431. D (-321) (-) m/ z 43.10 100.00% 43 71
5000 55 59 40 **———— । ... i TT
111.485 ..... "h 4.60 4.80 5.00 5.20 5.40 37 86 1' r ' " r " 11" " 11" 11" " I " " 111' m/z 71.10 92.93% mlz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #114555: 3-Buten-2-ol, 2-methyl- 43 7h 5000 . । .... । ic* A t *... 59 4.60 4.80 5.00 5.20 5.40 27 31 39 m/z 41.10 71.19%
/z-> mmmm 1518 + +so1561. -H 86 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 671 1.......................... 'I"
Abundance #114557: 3-Buten-2-ol, 2-methyl- 71 43 ■ i ■ ■ ■ 1 i ■ ■ 4.60 4.80 5.00 5.20 5.40 5000 m/Z 69.10 50.83% 59
27 31 39 53 50 53. 67 n/z—> "I...... ""I".......... |llli|ll.l|ilil|ll 11TTT—FLH 86 4i..........I1'-'-........ _______ L . A A___ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #24435: Butenol, methyl- ' ' 1 ' ' ' ' 1 ' ' ' 1 I ' ' r1 1 ' ' 43 71 4.60 4.80 5.00 5.20 5.40 m/z 55.10 34.97%
5000 59 27 15 31 39 53
n/z—> ...........12, 18 241 , | TTPmprtt TrtT | I I ,TJ I I I | 5 36, III|I I| + .46.50.1561, .63.67+ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ,74 79 8386 -AAAM44 4.60 4.80 5.00 5.20 5.40
08431.D SCAN020418.M Thu May 02 15:40:25 2002 Page 4
NYC-WTC_000048128
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NYC-WTC_000048169
Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048207
Laboratory report documenting GCMS analysis of sample AE08429 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048195
Laboratory report documenting GCMS analysis of sample AE08428 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048182
Laboratory report documenting GCMS analysis of sample AE08427 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048134
Laboratory report documenting GCMS analysis of sample AE08324 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048623
Gas chromatography-mass spectrometry results for sample AE08483 including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048106
Laboratory report documenting GCMS analysis of sample AE08323 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048647
Laboratory report documenting GCMS analysis of sample AE08486 conducted on May 7, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048635
GC/MS analysis report for sample AE08486 conducted May 7, 2002, detecting unknown compounds and surrogate standard 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048660
Laboratory report documenting GCMS analysis of sample AE08488 conducted on May 7, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047355
Laboratory report documenting GCMS analysis of environmental sample AE07513 conducted on April 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048672
Laboratory report documenting GCMS analysis of sample AE08489 conducted on May 7, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000048081
Department of Environmental Protection GCMS analysis record dated April 9-19, 2002.
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NYC-WTC_000048082
Fragmented document page containing metadata and identifiers related to GCMS testing procedures from early April 2002.
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NYC-WTC_000048085
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank run (Sample AE08323) from April to May 2002.
Filed in the same folder
NYC-WTC_000048094
Laboratory report of GCMS calibration (Sample AE08323) conducted between April 9 and May 3, 2002, showing response factors for volatile organics.
Filed in the same folder
NYC-WTC_000048098
Laboratory report of GCMS reference standard run (Sample AE08323) conducted between April 9 and May 3, 2002, verifying instrument performance.
Filed in the same folder