GCMS analysis results for sample AE08431, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020419\08431.D Vial: 18 Acq On : 20 Apr 2002 12:52 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 3-Penten-2-ol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

5.80 0.30 ug/1 429712 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-ol 86 C5H10O 001569-50-2 45 2 3-Penten-2-ol 86 C5H10O 001569-50-2 45 3 2-Butene, 1,4-dimethoxy- 116 C6H1202 026649-86-5 45 4 Furan, tetrahydro-2-(methoxymeth... 116 C6H12O2 019354-27-9 38 Abundance Scan 463 (5.799 min): 08431 .D (-459) (-) m/ z 41.10 100.00% 41 71

5000 ro 84 1 ' I ' ' ' - f i | i i rJ 1 51 '58-l l " pl. Iu‘BuIBIIaI1u*anyvi 5.40 m/ z 5.60 71.10 5.80 6.00 6.20 80.14% m/z-> 10 20 30 40 50 60 70I 80 90 100 110 120 Abundance #114530:3-Penten-2-ol 71 43

। । । । । /1 । 1 1 । Man 14 । Mw । 5000 53 5.40 5.60 5.80 6.00 6.20 27 m/z 43.10 69.98% 86

Tl/Z-> 1,113711, ■ i ' ' ' ' i 1 10 20 21 30 40 4459.571I1-1 1 180I 1 1e900 100 110 120 50 60 70

“Moem IAwNM Abundance #24376: 3-Penten-2-ol 43 71

5.40 5.60 5.80 6.00 6.20 5000 m/z 69.10 43.62% 27 53

n/z-> 15 -PP,# Hl 37, — 10 20 30 40 50 +41) 60 70I 80 86

90 100 110 120 Abundance #2798: 2-Butene, 1,4-dimethoxy- M... —A— 41 84 5.40 5.60 5.80 6.00 6.20 71 m/z 39.10 39.78%

5000 29 55

20 1 I 1 1 1 '1 ■' 1J 41,35-11111 KAI.,,. —11— ......... 98.............. 115 ............. ... ,4.18,4.. /z—> 10 20 30 40 50 60 I 8070 90 100 110 120 5.40 5.60 5.80 6.00 6.20

08431.D SCAN020418.M Thu May 02 15:40:27 2002 Page 5

NYC-WTC_000048129