GCMS results sample AE08255, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08255.D Vial: 13 Acq On 17 Apr 2002 7:22 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Muitiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 3-Penten-2-ol Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 5.68 0.31 ug/L 326864 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-ol 86 C5H10O 001569-50-2 59 2 3-Penten-2-ol 86 C5H10O 001569-50-2 43 3 Butanoyl chloride 106 C4H7C10 000141-75-3 38 4 1,6-Heptadien-4-ol 112 C7H120 002883-45-6 38 Abundance Scan 442 (5.676 min). 08255.D (-432) (-) m/z 43.10 100.00% 45 71

5000

53 co 84

n/z- > 0) 10 3& .......................... . 20 30 40 l2L+L ——p— 50 60 70 80 90 100 110 m/z 5.40 5 60 41.05 5 80 6 00 99.76% Abundance #114530: 3-Penten-2-ol 7h 43

5000 53 MAndeAan— + 5.40 5 60 5 80 6 00 27 m/z 71.10 96.89% 3& 58 86 ot 1 ■ i ' ,21 .11,1,733.77] 14844 +4 181____________ 1 65 1 ' 1 1 1 i 1 1 ' ' i P-■ । 1 1 ■ ■ i ■ Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #24376: 3-Penten-2-ol 43 7h

5.40 5 60 5 80 6 00 5000 m/z 39.10 57.30% 27 53

15 58 65 1 86 Ot --- 41 +44 I n/z- > Abundance 10 20 30 40

43 50 60 70 #6252: Butanoyl chloride 71 80 90 100 110 -4- 5.40 5.60 ... AM. ■ I ■ 1 ■ r I r , ’ 5.80 6 00 ■

27 m/z 69.10 52.17%

5000

78 0 -ll33.21 10 20 30 40 49 55 63 । ■ 1 'I 1'1 11 1 I 50 60 70 +19 80 90 ..... 100 106-110.. 5 40 5 60 5 80 6.00

08255.D 041702SCAN.M Thu Apr 18 09:24:57 2002 Page 8

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