GCMS results sample AE08255, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08255.D Vial: 13 Acq On 17 Apr 2002 7:22 pm Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Acetic acid, 3 -[1,3]dioxola... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.97 0.31 ug/L 328550 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3 -[1,3]dioxolan-2-y. .. 174 C8H14O4 1000186-02-3 36 2 Pentane, 3-methoxy- 102 C6H140 036839-67-5 17 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 12 4 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 Abundance Scan 492 (5 970 min): 08255 D (-483) (-) m/z 73.10 100.00% 73

5000 43 -------- 5 60 5.80 6.00 6.20 6 40 01 ............. 14.57 187.. 103........................ ■ ‘ I'' ■'I''1 ’I ’'1' I'1'1 lr'1 ’ I " 111' ' ' 1 I 1 1 " 1 1 " ' 1 1' '1 1 ’' ” I 1 1 "I" ’ 11 " ' ' I' 1 1 ' I "i qn.j p "IITET m/z 43.10 25.46% n/z- > 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25344 Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 5.60 5.80 6.00 6.20 6.40 43 m/ z 41.00 12.10% 27 55 . , 87 113 131 174 Tl/Z--> 0^ 1 H ।1111111" 11 -P '"I otg ' " I ' > " J vr> ' | t r i ' । t r i ■ । ' i i > । > । i r j । । r i । > । > i । 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25472 Pentane, 3-methoxy- 73 MMr, wenaq aMya 5.60 5.80 6 00 6.20 6.40 5000 m/ z 71.00 9.34% 45

29

n/z-> 0 " i11 ■ ■ i1 r 1 ■ r 0 10 20 1437, 55 30 40 ...I 101 ' i " ’ ’‘i' ' ' 1 "" ' । | i ' ' ' | i ' ' ' | i > " | i i ' 1 | r i r । j > i i । । > i i i । ■ । r > । 50 60 70 80 90 100 110 120 130 140 150 160 170 180 । ' i । ■ MoTn

Abundance #114826: Silane, tetramethyH 73 5 60 5 80 6 00 6 20 6.40 m/z 45.10 9.30% k 5000 A 43 15 29 2 || 53 65 0 11' I' -|mmmm n/Z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6 00 6 20 6.40

08255 .D 041702SCAN.M Thu Apr 18 09:24:57 2002 Page 9

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