Laboratory report documenting GCMS analysis of sample AE07632 conducted on April 9, 2002.
NYC-WTC_000047624–000047638Folder label: “GCMS X 4/4/02 A 4/15/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\020415\07632 .D Vial: 11 Acq On 15 Apr 2002 6:58 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C: \MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L
Peak Number 4 Acetic acid, 3-[1,3]dioxola.. . Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
5.97 0.51 ug/L 379065 1,4-Dichlorobenzene-d4 9.99
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 1000186-02-3 38 2 1,3-Dioxolane, 2-(3-bromo-5,5,5-... 352 C10H16BrC13O2 1000115-31-4 28 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 Abundance Scan 491 (5.964 min): 07632 D (-486) (-) m/ z 73.30 100.00% 73
5000 43 5 60 5.80 6.20 640 , 87 103 0- rI ' i "r1" i' r1 " r ■ " r "' r "' i " " r " ' i" ■ ■ i" m/ z 43.25 26.43% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25344: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester __ 73
5000 ' T / I*' ' r 5.60 5 80 6 00 6 20 640 43 m/ z 41.30 11.22% 27 —mmm 0- 111''1' r 55 . , 87 113 T11—0pmPTTemn 131 174 m/z-> Abundance
5000- 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #25473. 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dime 73 Mhs A I 5 60 m/ z —
5.80 45.30 A__ 6.00 6.20 8.96% 6.40
45
36 ll 55 ..........................109 ............................................................ 0- ------- TITPIPnTT Tl/Z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #857. N-Ethylformamide 3b 5.60 5 80 6 00 6.20 640 73 m/z 71.30 6.30% 5000 44 58
18 — /z- > 0 10 20 30 40 50 1—r i1 " ' i'11" । 60 70 80 " r " ' i " ■ ■ i H 1' I'' " r 1" I " " 11" 11111 '11" 1111 90 100 110 120 130 140 150 160 170 180 5 60 5.80 6.00 6.20 640
07632.D 041202SCAN.M Tue Apr 16 13:41:34 2002 Page 7
NYC-WTC_000047634
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NYC-WTC_000048436
GCMS analysis report for sample AE08269 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047867
GCMS analysis report for sample AE08255 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046757
Laboratory report documenting the GCMS analysis of sample AE08064 including surrogate recovery data and unknown compound screening on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048268
Laboratory report detailing surrogate recovery results for sample AE08260 analyzed on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047564
Laboratory report documenting GCMS analysis of sample AE07974 conducted on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046841
Laboratory report documenting GCMS analysis of sample AE08069 including surrogate recovery and unknown compounds on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046707
Laboratory report documenting the GCMS analysis of sample AE07978 including surrogate recovery data and unknown compound screening on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046740
Laboratory report documenting the GCMS analysis of sample AE08063 including surrogate recovery data and unknown compound screening on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046771
Laboratory report documenting the GCMS analysis of sample AE08065 including surrogate recovery data and unknown compound screening on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047577
Laboratory report documenting GCMS analysis of sample AE07975 conducted on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047535
Gas chromatography-mass spectrometry analysis of sample AE07972 documenting other unknown compounds and a 2,4-DDD surrogate recovery value of 76.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046799
Laboratory report documenting the GCMS analysis of sample AE08067 including surrogate recovery data and unknown compound screening on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000047510
Department of Environmental Protection GCMS analysis record dated April 4-15, 2002.
Filed in the same folder
NYC-WTC_000047511
Fragmented header page listing method parameters and quality control metrics for GCMS analysis.
Filed in the same folder
NYC-WTC_000047515
Laboratory report showing blank analysis results for sample AE07972 conducted between April 4 and April 15, 2002.
Filed in the same folder
NYC-WTC_000047525
Laboratory report displaying calibration data for sample AE07972 conducted between April 4 and April 15, 2002.
Filed in the same folder
NYC-WTC_000047528
Laboratory report displaying reference analysis data for sample AE07972 conducted between April 4 and April 15, 2002.
Filed in the same folder