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GCMS analysis results for sample AE07632, April 9, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07632 conducted on April 9, 2002.

NYC-WTC_000047624–000047638

Folder label: “GCMS X 4/4/02 A 4/15/02

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Scanned page image, NYC-WTC_000047635
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07632.D Vial : 11 Acq On : 15 Apr 2002 6:58 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

6.02 0.74 ug/L 556953 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 83 2 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 83 3 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 74 4 Acetic acid, 1,1-dimethylethyl e... 116 C6H1202 000540-88-5 36 Abundance Scan 501 (6 023 min): 07632 D (-497) (-) m/ z 43.30 100.00% 43

5000 59

101 MAN Ts । ■

+51 . II.... ..... 83| 5 60 5.80 6 00 6 20 6.40 0+ ........... 38 II m/z 59.30 39.94% n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #5851 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 5.60 5.80 600 6.20 6.40 59 m/z 58.3.0 21.92% ™ 101

n/z- > 0) --243239,4 10 20 30 40 48 53 67 72 77 83 91 96 । tpr ■•■‘I I ■ ■ ■ ■ i ■ ■ ■ ' i 1 1 1 1 1 1 1 1 -r ■' '' 1 1 1 50 60 70 80 90 100 110 Abundance #109755 2-Pentanone, 4-hydroxy-4-methyl- 43 0),.... . , , 5 60 5.80 6.00 6 20 6.40 5000 59 m/z 101.30 15.50%

15 31 101 0+ I, , 211, , 38,1 +534 I ' ' ' ' i 1 ' ' ■ i 83■ ' 1 i ' 1 1 Irr| 1 1 1 1 1 ■ > । > i ■ i । • 1 । । । 1 ' 1 pi n/z- > 10 20 30 40 50 60 70 80 90 100 110 Abundance #109756 2-Pentanone, 4-hydroxy-4-methy- 43 5.60 5.80 6.00 6.20 640 m/z 41.30 7.36% 5000 59

, 31 83 101 93 । 0 — ........ ■ 39,1 t-p ' '‘I I ■ ' ■ ■ f 1 ' 1 1 I 1 I ’ ' ' 1 I ‘ ' I ' 1/,%, 17 I —.Ah))) Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 5.60 5.80 6 00 6 20 6 40

07632.D 041202SCAN.M Tue Apr 16 13:41:36 2002 Page 8

NYC-WTC_000047635

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NYC-WTC_000047635Source: NYC Law Department, mirrored locally

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