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GCMS analysis results, Sample AE08262, April 22, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08262 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048309–000048332

Folder label: “GCMS X 4/9/02 A 4/17/02

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Scanned page image, NYC-WTC_000048324
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08262.D Vial: 19 Acq On : 18 Apr 2002 12:18 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98. L ******************************************** * * * * * * * * * * * ** ************ Peak Number 8 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.01 3.00 ug/L 2932100 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 72 2 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 43 3 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 40 4 Acetone______ 58 C3H60 000067-64-1 9 Abundance Scan 499 (6.011 min): 08262.D (-494) (-) m/z 43.05 100.00% 43

5000 59

101 5 60 5.80 6.00 6.20 6.40 71 83 119125 01 ............... —53 4 IPI—TIwuu"num m/z 59.10 41.21% r/z—> 10 ■ 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #109755. 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 I • ' 1 ' I ' ' 59 5.60 5 80 6 00 6 20 6.40 m/z 58.10 19.42% 15 101

n/z—> oJ — 10 20 ?53130 ,37,1 40 53, 1....... 11 11PPPTTT 50 60 70 80 83 90 100 110 120 130 Abundance #5851' 2-Pentanone, 4-hydroxy-4-methyl- 43 5 60 5.80 6.20 6.40 5000 m/ z 101.10 15.34% 59 101 04 ........ 27 377 53 I ' ' f-H- | 67 77 8,3 60 ' ' 70 ' ' 80 91 ' 90 j................................. 100 110 120 130 ' n/z-> 10 20 30 40 50 Abundance #109756: 2-Pentanone, 4-hydroxy-4-methyl- 43 5.60 5.80 6 00 6 20 6.40 m/z 41.05 4.79%

5000 59

101 83 93 . ........................... 0 _ ...... ..... ■ ■ i 1 ' 1 ' I ' 1 । i । . । . । । । । " I ' . ......... - 11 1— MWMMbcdMparn n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.60 5.80 6 00 6.20 6.40

08262.D 041702SCAN.M Thu Apr 18 09:49:32 2002 Page 13

NYC-WTC_000048324

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NYC-WTC_000048324Source: NYC Law Department, mirrored locally

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