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GCMS calibration results for volatile organics, April 2002

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Calibration data report for GCMS analysis of volatile organic compounds in sample AE08260 from April 2002.

NYC-WTC_000048256–000048259

Folder label: “GCMS X 4/9/02 A 4/17/02

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NYC 9/11 Public Portal Document

User: Nefliu, Marcela Westchester Dept, of Labs & Research Date: 04/19/2002 Time: 10:35:49

Sample: AE08260 Analysis: $C1GCMS CALI GCMS Units: ug Started: 4/9/02 10:33 Ended: 4/17/02 10:33 Analyst: MN Page: 1

Component Name* R Viol. .. Result i i Qualifier— MDL . 15 n-Nitrosodimethylamine 77 2.0

12 23, bis(2-Chloroethyl)ether 1,3-Dichlorobenzene 73 75 2.0 2.0 4 1,4-Dichlorobenzene 74 2.0 1 5 1,2-Dichlorobenzene 71 2.0 ; 6 2,2‘-oxybis( 1 -Chloropropane) 78 2.0 7 n-Nitrosodi-n-propylamine 76 2.0 8 Hexa chloroethane 74 2.0 49. Nitrobenzene 74 2.0 10 Isophorone 73 2.0 11 bis(2-Chloroethoxy)methane 75 2.0 <12 1,2,4-T richlorobenzene 76 2.0 13 Naphthalene 73 2.0 '14 Hexa chlorobutadiene 66 2.0 15 2-Chloronaphthalene 81 2.0 116 Dimethylphthalate 86 2.0 17 2,6-Dinitrotoluene 81 2.0 18 Acenaphthylene 77 2.0 219 Acenaphthene 77 2.0 20 2,4-Dinitrotoluene 98 2.0 ; 21 Diethylphthalate 83 2.0 ’ 221 4-Chlorophenylphenylether 82 2.0 234 Fluorene 78 2.0 24. Azobenzene 80 2.0 725 ' n-Nitrosodiphenylamine 78 2.0 2 26 i 4-Bromophenylphenylether 63 2.0 27. Hexa chlorobenzene 59 2.0 28 4 Phenanthrene 74 2.0 29; Anthracene 75 2.0 302 Di-n-butylphthalate 76 2.0 311 Fluoranthene 76 2.0 32V Pyrene 86 2.0 330 Butylbenzylphthalate 93 2.0 134 Benzo(a)anthracene 83 2.0 35 bis(2-Ethylhexyl)phthalate 99 2.0 36 Chrysene 83 2.0 374 Di-n-octylphthalate 78 2.0 38 5 Benzo(b)fluoranthene 78 2.0 39); Benzo(k)fluoranthene 70 2.0 40; Benzo(a)pyrene 74 2.0______

437 lndeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene 43 Benzo(g ,h ,i)perylene 80 91 84 2.0 2.0 2.0

NYC-WTC_000048256

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NYC-WTC_000048256Source: NYC Law Department, mirrored locally

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