NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\l\DATA\020415\0404LB.D Vial : 8
Acq On 15 Apr 2002 4:29 pm Operator: Nefliu
Sample 04/04 lab blk Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator)
Title 508 Modified GC/MS scan
Library C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 1 Acetic acid, 3- [1,3]dioxola. .. Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
5.97 0.54 ug/L 410466 1,4-Dichlorobenzene-d4 9.99
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Acetic acid, 3- [1,3]dioxolan-2-y... 174 C8H14O4 1000186-02-3 28
2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 12
3 Silane, tetramethyl- 88 C4H12S1 000075-76-3 9
4 N-Ethylformamide 73 C3H7NO 000627-45-2 9
Abundance Scan 491 (5 964 min) 0404LB D (-486) (-) m/ z 73.30 100.00%
73
5000
43
1 i ■ ' ■ ■ i ■ ■
55 5.60 5.80 6 00 6.20 6.40
n/z->
0- 1" ।" "i i ■1" । +4 1 87 103
r " 11" " i' "" i11 i' H11 r' " i1" ' i " " i'1" r 111 r 1" r " 11" " i ■ ■
0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180
m/ z 43.30 24.72%
Abundance #25344: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester
73
5000 . AA, ।
5.60 5 80 6.00 6.20 6.40
43 m/ z 41.30 11.52%
n/z->
0- TITTTT
0
27
R +TT 87
10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180
113 131 174
' i' ‘ " r " ■ r " ' r " ' r1" I'1
Abundance #25349 Silane, tetramethyl-
73
-
5.60 5 80 6 20 6.40
5000 m/ z 45.30 10.31%
no 43
0- 112 .. 15.. 2.. 11 55.65 I.... 88...................................................
111" i1111111 FT’1111' 111"1 ’ i" " r' ’ . । ... । | rr. . । ’T’’ I’l । ।i i । 11 । i । 11 < । । । ।
n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180
Abundance #114850 Silane, tetramethy-
73 5 60 5.80 6.00 6.20 6.40
m/z 71.30 6.65%
5000
45
0 29 37 IITTTTTTT
59
MU
1 '1....... 1....... । ■'1 ■ । 1 r''11" ■ ‘ i
/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5 80 6.00 6 20 6.40
0404LB.D 041202SCAN.M Tue Apr 16 11:54:18 2002 Page 4
NYC-WTC_000047521
OCR can misread numbers and units. Confirm readings against the page image before using them.