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GCMS analysis results, Sample AE08265, April 22, 2002

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GCMS analysis report for sample AE08265 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048378–000048400

Folder label: “GCMS X 4/9/02 A 4/17/02

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Scanned page image, NYC-WTC_000048391
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08265.D Vial: 22 Acq On : 18 Apr 2002 2:44 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Acetic acid, 3- [1,3]dioxola... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

5.96 0.35 ug/L 394092 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y. . . 174 C8H14O4 1000186-02-3 33 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 12 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 N-Ethylformamide 73 C3H7NO 000627-45-2 9 Abundance Scan 491 (5.964 min) 08265.D (-486) (-) m/z 73.10 100.00% 73

4 5000 43 5.60 5.80 6.00 6.20 6.40 87 n/z-> 0^ —0 .10........ 11,55,.. 4 PIU—mnmmPPIWTTT | 103

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/ Z 43.10 26.38% Abundance #25344: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 ----- rp-rrTIu 5 60 5 80 M 6.00 6.20 TT 640 43 m/z 41.10 10.65% 27 55131 87 174 0 m-T r ■ " i " ■11' I i" " i " " 113 i'1"i" "r 11' i" " r ' " i ” " r1 " i " n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25349 Silane, tetramethyH- 78 AAadnhaCMeuduaup 5 60 5.80 6.00 6.20 6 40 5000 m/z 45.00 10.07%

no 43

/z-> 0 2 15/28.155,65, ■IT | 'I II I | J fl I | I I "ITTTUrmmtir’ TT 0 I 111 ■■111■" 111"11" ■ ।1'1 'I''1' i'1111'1111"111H1 • i'1

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #114850: Silane, tetramethyl- .................... 1................ 73 5 60 5 80 6.00 6.20 6.40 m/ z 71.10 6.40% 5000

45 0 ".......... 29371 ’TCCCII—ITIT"T’’TT 59 . ... ...................................................... 11'‘'‘'‘'T" " I' ’ ’0"’11001U0V00TUT"ITUTTTTTTTTT"TOOOOT"TTTT’TTTT’T 4 . .. 14... pp1—7 n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5 60 5.80 6 00 6.20 6.40

08265.D 041702SCAN.M Thu Apr 18 09:58:14 2002 Page 10

NYC-WTC_000048391

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NYC-WTC_000048391Source: NYC Law Department, mirrored locally

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