GCMS analysis results, Sample AE08265, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \MSDCHEM\1\DATA\020417\08265.D vial: 22 Acq On : 18 Apr 2002 2:44 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 2-Propanone, 1,1,1-trichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.03 0.71 ug/L 794010 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 42 2 Butanoic acid, 2-acetyl-3-methyl... 158 C8H14O3 051756-10-6 9 3 1-Fluorononane 146 C9H19F 000463-18-3 9 4 .beta.-d-Fructofuranose, 1,3,4-t... 288 C12H1608 1000151-08-8 9 Abundance Scan 502 (6.029 min): 08265.D (-497) (-) m/z 43.05 100.00%| 43

5000

p/z-> 01 ■ ■ । 35 । ।1' 11 ’p’r 111' 10 20 30 40 50 i5PRR7r - 11711 60 70 82

80 90 97 I'' ’ I’ " 1 I'''' I 100 110 120 130 140 150 160 i11111'1 5.60 m/z 124.90 5.80 6.00 6.20 6.40 9.91% Abundance #3877 2-Propanone, 1.1,1-trichloro- 43

- 5000 5.60 5 80 6 00 6.20 6.40 m/z 47.00 6.99% 15| 27 36 __ ol TTTT 1 ' ''I ' ■ 1 ' I1' ,50 63 76 83 97 110117 125 ■ | । i 1 । | ITr TPWTNTUTTP I ' ' • ' I 1 ‘ n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance ■tni55 Butanoic acid, 2-acety/3-methy-, methyl ester 43 MWNw 101 5.60 5.80 6 00 6.20 6.40 5000 m/z 126.90 6.71% 116 15 69 27 84 127

n/z- > 01 TTpr 10 -4 . 51,5% mm 20 30 40 '' ’ I ■'1 ■ I' 50 I i ■ • ■ ■ i 143 158 i ■'' ' i11' ■ i'' 60 70 80 90 100 110 120 130 140 150 160 Abundance #4248: 1-Fluorononane ................................. .............. .. 43 5.60 5.80 6.00 6.20 6.40 m/z 97.00 5.50% 55 5000 29 70 84 97

Tl/Z—> 15 0 '' I ‘ 1 1 1 I ' 10 20 +36 ++ +42-774 30 40 50 60 701 80 104111118 126 tht 1 90 ' I'" " I " " I 146 i''' ■ i ■ • ■ ■ i'1 100 110 120 130 140 150 160 ................................. 5 60 5.80 6.00 6.20 6.40

08265.D 041702SCAN.M Thu Apr 18 09:58:16 2002 Page 11

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