GCMS analysis results for sample AE08065, Apr 2002

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Library Search Compound Report

Data File : C : \MSDCHEM\1\DATA\020415\08065.D Vial: 22 Acq On : 16 Apr 2002 3:59 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 5 2-Propanone, 1,1,1-trichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.04 0.66 ug/L 558133 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 45 2 Sulfurous acid, dipropyl ester 166 C6H14O3S 000623-98-3 9 3 2-Propanone, 1,1-diethoxy- 146 C7H14O3 005774-26-5 9 4 .beta.-d-Fructofuranose, 1,3,4-t... 288 C12H1608 1000151-08-8 9 Abundance Scan 503 (6 035 m.n) 08065.D (-498) (-) m/ z 43.30 100.00% 43

5000

35 E4 59 83 97 125 5 60 . A .. u-mTTITr 5.80 6.00 6 20 6.40 +l 0+ "I'1 '1 1 ' ' 11 11 Irll i., 117 II m/z 125.10 9.58% n/z—> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 #3877 2-Propanone, 1.1,1-trichloro- I 43

5000 5 60 5 80 6 00 6.20 6 40 m/z 127.20 7.94% 15 97

0+ । I' I11.......... I27 36 | I 1 ,50 1!,. .'I', 63 76 83 97 110117 125 । ■ ■ ■ 'T1-11111' Ui1111 r1'1 ■ ■ । ■1 ■ ।111 ■ pmhdg"1 *. ... 1 • ■ n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #109140 Sulfurous acid, dipropyl ester 43 5 60 5.80 6.00 6 20 6.40 5000- m/z 97.20 6.17% 27

n/z- > 0+ ..... BX?, T1muun 10 . 59 6 6 73 83 20 30 95 107 i-|5 125 137 —,BO0‘0gumpr 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #4951 2-Propanone, 1,1-diethoxy- 43 5 60 5 80 6 00 6 20 6.40 m/z 83.20 5.89% 5000

29 75 101 18 87 0 4 14136.4 51 59 68 '80mlp90 — 108 115 129 137144 Ir ' ' i ■ ■ 141 rP*I 1 ।' iii l ; Tl/Z-> 10 20 30 40 50 60 70 100 110 120 130 140 150 5 60 5 80 6.00I 6 20 6.40

08065.D 041202SCAN.M Tue Apr 16 13:54:45 2002 Page 8

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