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GCMS analysis results for sample AE08065, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting the GCMS analysis of sample AE08065 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046771–000046785

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08065.D Vial: 22 Acq On : 16 Apr 2002 3:59 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 6 Phenanthrene, 9-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.24 ug/L 331691 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 45 3 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 40 4 2-Imidazolidinone , 1-methoxy-3-p.. . 192 C10H12N2O2 052420-43-6 37 Abundance Scan 3330 (22 645 min): 08065.D (-3322) (-) m/z 192.30 100.00% 192

5000

1 1 i ■ ' ■ ' i 1 1 1 1 i ' ' 82 96 146 160 22.40 22 60 22 80 23.00 ■ i " " r 42 , (, . HI hI , , H,lI. j. mpmmmmptp I. H 70 120 I, 1 ’ I ’I m/z 191.30 19.83% /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene. 9-methyl- 192

5000 22.40 22 60 22 80 23.00 m/z 146.30 13.94%

n/z- > 29 39 51 63 75 83 0- ' i " " i " ■' i ■ ■ ■' i ' ■ ■ ■ i ''■ ■ ■ i ■11 ■ i1 ■ ■ 96 —L115,126,139.152.1176 4 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 165 i । '' r ■ fl Abundance #80950: 1,5-Naphthalenedithiole 19 2 A . I I II I

22.40 22 60 22.80 23.00 5000 m/z 193.30 13.56% 115 128 159 40 57 69 79 96 , 147 ov ... . , r. .'J, +4 444.87,1. 19f Al. ,, +136,l —177. /Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870 Thiocyanic acid, 2-benzothiazolyl ester 192 22,40 22.60 22 80 23.00 m/z96.20 11.16% 5000

69

n/z-> ov H 45 ------mmmmm— mH 82 90 ’’| ’T 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 108 122 134 -148 160 I'''' I ,,1,1.............. 22 40 22 60 22 80 23 00 1,

08065.D 0412 02SC7VN. M Tue Apr 16 13:54:45 2002 Page 9

NYC-WTC_000046783

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NYC-WTC_000046783Source: NYC Law Department, mirrored locally

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