GCMS analysis results for sample AE08063, Apr 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08063.D Vial: 20 Acq On : 16 Apr 2002 2:21 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 7 2-Propanone, 1,1,1-trichloro- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

6.04 0.68 ug/L 585692 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 42 2 2-Propanone, 1,1 -dichloro- 126 C3H4C120 000513-88-2 25 3 2-Propanone, 1,1 -dichloro- 126 C3H4C12O 000513-88-2 9 4 1-Eicosanol 298 C20H42O 000629-96-9 9 Abundance Scan 503 (6 035 min)' 08063 D (-498) (-) m/ z 43.30 100.00% 43

5000 , . ........................... .... 5 60 5 80 6 00 6 20 6 40 35 .49.59... ... ... 117 125 ol 1—— r 1 f | ■ l ■ r | . . > r | I >. . | | f ( 1 ' I ' ' ' 1 I ' 1 ' 1 I ‘ ' 1 'I 1 ' ' ' I ' m/z 125.20 8.91% n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3877 2-Propanone, 1,1,1-trichloro- 43

5000 5 60 5 80 6 00 6.20 6.40 m/z 127.20 6.52%

n/z-> Ot IP 10 15 |

20 27

30 36

40 49 55 63 +m —m—m 50 76 83 91 97 mma 60 110 117 1 25 70 80 90 100 110 120 130 A Abundance #3861 2-Propanone, 1.1-dichloro- 43 5.60 5.80 6.00 6.20 6.40 5000 m/z 97.10 6.33%

15 27 I I 36 1 ‘49 55 63 7 6 83 93 1 25 04 PP I’) ..I । । ■ 1 ' । ‘‘ ■ 1‘ । ( । । ■ Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #109152 2-Propanone, 1,1-dichloro- 43 5 60 5 80 6 00 6 20 6.40 m/z 83.10 5.39%

5000-

27I , 49 55 63 76 83 91 30 111 126 0 1 ,'l'l ' 1 ■ ■ i 1 ' i 1 ' 1 1 i ■■ i ' ■ ■ ■ । । i'1 > । 1 1 1 ITIIIU’I | 1 । n/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5 60 5 80 6.00 6.20 6.40

08063.D 041202SCAN.M Tue Apr 16 13:51:58 2002 Page 10

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