GCMS analysis results for sample AE07977, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\l\DATA\020415\07977.D Vial : 17 Acq On 15 Apr 2002 11:54 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L Peak Number 6 2-Propanone, 1,1,1-trichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.05 1.02 ug/L 905849 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 42 2 2-Propanone, 1,1 -dichloro- 126 C3H4C120 000513-88-2 9 3 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 4 1-Nonadecanol 284 C19H40O 001454-84-8 9 Abundance Scan 505 (6 046 min): 07977.D (-500) (-) m/ z 43.30 100.00% 43

5000

rTrTtr IT’’ 83 97 125 5 80 6.00 6.20 6.40 35 61 0+ IPPTTT 49 ■ । । ■ ■ ■■ r1 ■ 1 ■ । 1 -H I । 110 119 II m/z 125.20 10.88% n/z-> 10 20 30 40 50 60 70 80 !90 100 110 120 130 Abundance #3877 2-Propanone, 1,1,1-trichloro- 43

.......... , ........... 5000 5.80 6.00 6.20 6.40 m/z 127.20 6.87%

n/z-> 15 | 01 ........ . 10 27 36 49 55 63 76 83 91 97 110 117 125 I " Iei ' ■‘<•■-11 1 ‘ ri ■ ■ • ■ r1''1 ■ i1 ■ । ■ ।11,11 ■ ■ ’’i 11 ■. ।.... pi >'i*i 111 20 30 40 50 60 70 80 90 100 110 120 130 1 Abundance #109152: 2-Propanone, 1,1-dichloro- 43 5 80 6 00 6 20 6.40 5000- m/ z 97.20 6.07%

27 . 49 55 63 76 83 91 1 3b 111 126 0+ ' ' I ' ' 1 ' I 1 1 IH) 1 ItHIl 11’FI ■1 ■ ■ i। ■111,,,,, 11‘1 ■ >' ।r 1111111 ■ ।1 ■ ■1111 Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3861: 2-Propanone, 1,1-dichloro- ■ ■ । ■ ———————— 43 5.80 6.00 6 20 640 m/ z 83.20 5.84% 5000 4 15 27 1 49 55 63 1 36 +P 76 83 93 125 0 11+ n/z— > 10 20 30 40 50 60 70 80 90 100 110 120 130 580 6 00 6.20 6.40

07977.D 041202SCAN.M Tue Apr 16 13:47:09 2002 Page 9

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