GCMS analysis results for sample AE07977, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07977.D Vial: 17 Acq On : 15 Apr 2002 11:54 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 7 Phenanthrene, 9-methyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.22 ug/L 306281 Phenanthranene -dl0 23.02

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 42 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42 4 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 42 Abundance Scan 3330 (22.645 min) 07977 D (-3322) (-) m/z 192.30 100.00% 19 2

5000-

96 146 160 22.40 22.60 22.80 23.00 40 49 70 82 118 0-T TTTTT-H—t ............ If"' - m/z 191.30 22.37% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyH 192

5000 -- TI 22.40 22.60 22.80 23.00 m/Z 193.30 19.53% 96 1 65 i i

n/z-> ov BIWnmumgmn 29 39 51 63 75 83 .115, 126,139,152.1176 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ■ ■ ।r >

Abundance #125844 Anthracene, 2-methyl- 19 2

22 40 22 60 22 80 23.00 5000 m/z 146.30 14.58%

92 96 1 65 .........................63 J4 £ |........ 115......... 139 150..... 1176, 0- i11'11 ■11 ■ । " r " 11" " I.. 11 ITTi’’ '11111 rr tumn n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125848: Anthracene, 9-methyl- 19 2 22.40 22.60 22.80 23.00 m/z 96.20 13.02% 5000

N 96 115 126 139 152 165 Tl/Z-> 27 3 9 51 63 74 82 1 0-T PUTPTTTPTTTTTTTT mTmTTTT 0 176 . 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 n 11 2240 22 60 22 80 23 00

07977.D 041202SCAN.M Tue Apr 16 13:47:10 2002 Page 10

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