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GCMS analysis results for sample AE07977, April 18, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07977 conducted on April 18, 2002.

NYC-WTC_000047608–000047623

Folder label: “GCMS X 4/4/02 A 4/15/02

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Scanned page image, NYC-WTC_000047622
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020415\07977.D Vial: 17 Acq On : 15 Apr 2002 11:54 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 8 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.39 ug/L 543308 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 94 (2) Phenanthrene-dlO 188 C14D10 001517-22-2 72 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 40 4 Pentacyclo[7.3.1.1. (4,12) .0(2,7) ... 188 C14H20 1000215-61-8 36 Abundance Scan 3420 (23.174 min). 07977 D (-3413) (-) m/z 188.40 100.00% 108

5000

, 5 66 80 94 . ........................ ........... 22 80 23 00 23.20 23.40 23 60

TVz-> 0 ........... 13.52... 1.... l-ull. ull. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z189.40 15.42% Abundance #79826. Anthracene-d10- 118

5000 Tr ,|~i 1 1 1 1 i ' 1 22 80 23 00 23.20 23.40 23 60 80 94 m/z 184.30 13.64% 160 , I 17 30 42 52 66 n/z—> 0 + . | 102 TTmum 118 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 132 146 +170.1894. Abundance #79827. Phenanthrene-d10 188

22 80 23 00 23 20 23.40 23.60 5000 m/z 94.30 11.86%

80 94 160 30 42 52 66 n/z-> | 102110118 132 146 0- BAAyunvogoovoptasap+soptugaoum Ui | 1 I I TTTrrt I I I | I I I I | I I I , | ! I i i

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 -701894... Abundance #125696' 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime ‘I***I*ITum/II‘III‘ 188 22 80 23.00 23.20 23.40 23.60 m/z 8.0.25 9.70% 5000 143 . 89 115 170 51 76 | 102 I. 130।mll K| > I158 ti/z-> 0 -- I I |'l I l r. 111" 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 U ' i 1 1 ' ■ i 22.80 23 00 23.20 1 1 1 1 1 I 23.40 23.60

07977 .D 041202SCAN.M Tue Apr 16 13:47:10 2002 Page 11

NYC-WTC_000047622

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NYC-WTC_000047622Source: NYC Law Department, mirrored locally

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