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GCMS analysis results for sample AE07979, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE07979 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046722–000046739

Folder label: “GCMS X 4/5/02 A 4/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07979.D Vial: 19 Acq On : 16 Apr 2002 1:32 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 10 Anthracene-dlO - Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.31 ug/L 383312 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 72 27 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 33 4 Antipyrine 188 C11H12N2O 000060-80-0 28 Abundance Scan 3420 (23 174 mm) 07979 D (-3415) (-) m/z 188.40 100.00% 168

5000

94 40 66 80 . 156 22 80 23 00 23 20 23.40 23.60 146 11 ov -PH ................................... .. ...i" .... m/z 94.30 19.10% /Z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826 Anthracene-d10- 188

5000 22 80 23 00 23 20 23 40 23.60 m/z 189.30 16.39% 80 94 160 । I 66

n/z-> 17 30 42 52 118 132 146 Qi IITTTP . । i. 11 > 111111 ■ r11.1 ■■11 TWPITTTTTTTTT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 +..179.189.. Abundance #79827 Phenanthrene-d10 108

22 80 23 00 23 20 23.40 23 60 5000 m/z 184.30 12.89%

80 94 160 30 42 52 66 n/z- > 01'I" "I ""I" "I ""I1'"'l'11.11 il-ll1" 0 4102110118.182,146,44470.149/, — 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 22 80 23.00 23 20 23.40 23.60 m/z 92.20 8.90% 5000 143 . 89 115 51 64 76 | 102 । 130 , 158 170 0 ------------ -HHH Tr n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23 00 23.20 23.40 23.60

07979.D 041202SCAN.M Tue Apr 16 13:48:32 2002 Page 13

NYC-WTC_000046738

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NYC-WTC_000046738Source: NYC Law Department, mirrored locally

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