GCMS analysis results for sample AE08067, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE08067 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046799–000046812

Folder label: “GCMS X 4/5/02 A 4/16/02”

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Data File : C:\MSDCHEM\1\DATA\020415\08067.D Vial: 24 Acq On : 16 Apr 2002 5:36 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 23.17 0.38 ug/L 323710 Phenanthranene-dl0 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 78 2 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 40 3 Benzaldehyde, 2,5-difluoro-4-hyd ... 188 C8H6F203 148872-77-9 40 4 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N2O2 005603-22-5 40 Abundance Scan 3420 (23.174 min). 08067 D (-3414) (-) m/z 188.35 100.00% 18 8

5000

94 40 49 57 66 80 --mP 156 । 22 80 23 00 23.20 23 40 23.60

n/z- > 0- +ml.. --mll— 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 tv m/z 184.35 18.81% Abundance #79826: Anthracene-d10- K8

5000 22 80 23.00 23 20 23.40 23.60 m/z 94.30 17.00% 80 94 160 , I 66 17 30 42 52 118 132 146 ,i| 170 180 । 01 ■ I ■< I ■ I" 11 ............... 111 'l‘lT''' ।,"'' 111)11 UTIII n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79801: 2,2.9.9-Tetramethyldec-5-ene-3,7-diyne 188 173 41 131 143 22 80 23 00 23 20 23 40 23 60 91 5000 77 158 m/z 189.30 13.25% 57 119 27 67 105

01 pm Hl l-l — IL k u n/z—> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #79822 Benzaldehyde, 2.5-difluoro-4-hydroxy-3-methoxy- 1 8 . ... H,. ... ...... 22 80 23.00 23.20 23.40 23.60 m/z 40.20 9.79% 5000

n/z-> 0- 41 49 57 69 77..88, 97, 109117 12813705 159 ..... TT । I’ ... 11 I l'l| . ‘ ‘‘ , | "T* i'h । । "CTTTTTTTuuT’ i i i । rri ,|-i i 1 Wn 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TTT i ■ ■ ■ 1 i ■ 22 80 23 00 23.20 23.40 23.60

08067.D 041202SCAN.M Tue Apr 16 13:56:08 2002 Page 9

NYC-WTC_000046811

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NYC-WTC_000046707

Laboratory report documenting the GCMS analysis of sample AE07978 including surrogate recovery data and unknown compound screening on April 18, 2002.

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