GCMS analysis results for sample AE08067, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE08067 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046799–000046812

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \MSDCHEM\1\DATA\020415\08067 .D Vial: 24 Acq On 16 Apr 2002 5:36 am Operator: Nefliu Sample sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Phenanthrene, 9-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 22.64 0.22 ug/L 185092 Phenanthranene-dl0 23.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Thiophene, 2-[2 -(3-thienyl)ethen. . . 192 C10H8S2 116854-09-2 40 3 1,5 -Naphthalenedithiole 192 C10H8S2 1000223-69-5 38 4 Bitoscanate 192 C8H4N2S2 004044-65-9 38 Abundance Scan 3330 (22 645 min) 08067.D (-3324) (-) m/z 192.30 100.00% 192

5000

. ..... n,, 42 66 82 96 146 160 I 22.40 22 60 22.80 23.00 0 <।1>■■।■■■■i 'i'>>>।।।/1 । 1■ A ।It..। ■ ।।11 ’111"1111 pokoan i" 1111 ri।|"l.,।, m/z 191.30 20.42% /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033 Phenanthrene, 9-methy- 1'2

5000 .........11...... 1, 22 40 22.60 22 80 23.00 m/z 146.30 15.25% 96 165 i । 51 63 75 83 | 115 126 139 152 , 176 Ot "29r '''39r 11**—** "i" n/z— > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81023: Thiophene, 2-(2-(3-thienyl)ethenyl]- 1,2 1 1 i 1 ' ' ) 1 1 i ■ ■ 147 22 40 22 60 22.80 23.00 5000 m/z 193.20 15.25% 45 A 5o 69 96 115 134 n/z-> 27 37 .1211787,110511 P i purlpor 158 ...177. Im 0 TITTTH i | ri । ‘1116 r| rf rr| “ t ri “i I r I j 11 ! 11 ITT I | I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80950: 1,5-Naphthalenedithiole "h T‘ 1 । 1 r । ' 1 1 i ' 1 1'2 22.40 22 60 22 80 23 00 m/z 96.30 12.21% 5000 159 I 115 128 A 40 57 69 79 96 147

n/z-> 0 -rp-r 20 ----- 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 136,4— 177i' ।' ‘ i'll "i" ‘ i1 • 22.40 22 60 22.80 23.00

08067.D 041202SCAN.M Tue Apr 16 13:56:08 2002 Page 8

NYC-WTC_000046810

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NYC-WTC_000046707

Laboratory report documenting the GCMS analysis of sample AE07978 including surrogate recovery data and unknown compound screening on April 18, 2002.

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